Calibration standard analysis results, sample C5, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\050102\C5A0501.D Vial: 8 Acq On 1 May 2002 ■ 5:33.pm Operator: Bohlk / Inst 213 Sample C5 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: May 06 12:52:27 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Mon May 06 12:42:26 2002 Response via : Initial Calibration DataAcq Meth : 050102

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 17.59 164 3914658 5.00 ug/L 0.00 9) Phenanthrene d-10 21.89 188 5585789 5.00 ug/L 0.00 19) Chrysene d-12 29.62 240 3972466 5.00 ug/L 0.00 25) p-Terphenyl d-14 26.77 244 3520853m 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 12.55 134 876941 4.90 ug/L. 0.00 Spiked Amount 5.000 Recovery = 98.00% 20) Triphenyl Phosphate 28.94 326 937635 5.30 ug/L 0.00 21) Perylene D-12 33.60 264 2933536 5.31 ug/L 0.00 Spiked Amount 5.000 Recovery = 106.20% 26) Acenaphthene d-10 (surr) 17.59 164 3914658 4.47 ug/L 0.00 Spiked Amount 5.000 Recovery = 89.40% 27) Phenanthrene d-10 (surr) 21.89 188 5585789 4.68 ug/L 0.00 Spiked Amount 5.000 Recovery = 93.60% 28) Chrysene d-12 (surr) 29.62 240 3972466 5.01 ug/L 0.00 Spiked Amount 5.000 Recovery = 100.20%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 15.11 237 511719m 4.73 ug/L 4) Hexachlorobenzene 20.76 284 1263735m 5.17 ug/L 5) EPTC 15.60 128 1898386m 5.10 ug/L 6) 2,6-Dinitrotoluene 17.18 165 775050m 4.77 ug/L 7) 2,4-Dinitotoluene 18.32 165 634371 4.42 ug/L 98 8) Molinate 18.48 126 2804220 5.03 ug/L 98 10) Simazine 21.33 201 650728 4.82 ug/L 100 11) Atrazine 21.45 200 1174144 4.84 ug/L 92 12) Alachlor 23.29 160 1263098 4.94 ug/L 94 13) Terbacil 22.28 117 505446 4.80 ug/L 96 14) Acetochlor 23.08 146 898167 4.78 ug/L 93 15) Metribuzin 23.11 198 1242241 4.88 ug/L 96 16) Metolachlor 24.21 162 3853913 5.06 ug/L 91 17) Butachlor 26.03 160 1002365 4.77 ug/L 97 18) 4,4'-DDE 26.66 246 1168977 5.03 ug/L 90 22) Bis (2-Ethylhexyl) adipate 28.90 129 2130589 4.42 ug/L 91 23) Bis (2-Ethylhexyl) phthala' 30.32 149 3796640 4.62 ug/L 92 24) Benzo (a) pyrene 33.44 252 3229871 4.28 ug/L 95

(#) = qualifier out of range (m) = manual integration C5A0501.D 050102.M Mon May 06 12:53:48 2002 Page 1

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