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← Document results/DEP Box 65/525 X 4/30/02 A 5/1/02
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Reference standard analysis results, sample AE10186, May 2002

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Results for reference standards including hexachlorobenzene and alachlor analyzed between April 30 and May 2, 2002.

NYC-WTC_000082548–000082580

Folder label: “525 X 4/30/02 A 5/1/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\050202\10186.D Vial: 22 Acq On 2 May 2002 6:59 pm Operator: Bohlk / Inst 213 Sample SAMPLE 10186 4/30/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: May 06 14:51:13 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Mon May 06 12:42:26 2002 Response via : Initial Calibration DataAcq Meth : 050102

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 17.59 164 2913211 5.00 ug/L 0.00 9) Phenanthrene d-10 21.89 188 4871653 5.00 ug/L 0.00 19) Chrysene d-12 29.62 240 3215392 5.00 ug/L 0.00 25) p-Terphenyl d-14 26.77 244 3832692m 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 12.55 134 756556 5.68 ug/L 0.00 Spiked Amount 5.000 Recovery = 113.60% 20) Triphenyl Phosphate 28.94 326 841959 5.88 ug/L 0.00 21) Perylene D-12 33.60 264 362876 0.81 ug/L 0.00 Spiked Amount 5.000 Recovery = 16.20% 26) Acenaphthene d-10 (surr) 17.59 164 2913211 3.05 ug/L 0.00 Spiked Amount 5.000 Recovery = 61.00% 27) Phenanthrene d-10 (surr) 21.89 188 4871653 3.75 ug/L 0.00 Spiked Amount 5.000 Recovery = 75.00% 28) Chrysene d-12 (surr) 29.62 240 3215392 3.72 ug/L 0.00 Spiked Amount 5.000 Recovery = 74.40%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 'N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 0.00 126 0 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 117 0 N.D. 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 0.00 129 0 . N.D. d 23) Bis (2-Ethylhexyl) phthala 30.31 149 70821m 1.39 ug/L 24) Benzo (a) pyrene 0.00 252 0 N.D.

(#) = qualifier out of range (m) = manual integration 10186.D 050102.M Mon May 06 14:53:20 2002 Page 1

NYC-WTC_000082551

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NYC-WTC_000082551Source: NYC Law Department, mirrored locally

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