Calibration standard analysis results, sample C5, May 2002

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Results for calibration standards including deuterated compounds analyzed on May 6, 2002.

NYC-WTC_000082506–000082517

Folder label: “525 X 4/30/02 A 5/1/02”

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Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\050102\C02A0501.D Vial: 4 Acq On 1 May 2002 2:30 pm Operator: Bohlk / Inst 213 Sample CO .2 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: May 06 13:07:08 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Mon May 06 12:42:26 2002 Response via : Initial Calibration DataAcq Meth : 050102

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 17.59 164 3658427 5.00 ug/L 0.00 9) Phenanthrene d-10 21.89 188 5037935 5.00 ug/L 0.00 19) Chrysene d-12 29.62 240 3658766 5.00 ug/L 0.00 25) p-Terphenyl d-14 26.77 244 3271834m 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 12.55 134 900814 5.39 ug/L 0.00 Spiked Amount 5.000 Recovery = 107.80% 20) Triphenyl Phosphate 28.94 326 645807 3.96 ug/L 0.00 21) Perylene D-12 33.60 264 2294877 4.51 ug/L 0.00 Spiked Amount 5.000 Recovery = 90.20% 26) Acenaphthene d-10 (surr) 17.59 164 3658427 4.49 ug/L 0.00 Spiked Amount 5.000 Recovery = 89.80% 27) Phenanthrene d-10 (surr) 21.89 188 5037935 4.54 ug/L 0.00 Spiked Amount 5.000 Recovery = 90.80% 28) Chrysene d-12 (surr) 29.62 240 3658766 4.96 ug/L 0.00 Spiked Amount 5.000 Recovery = 99.20%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 20.77 284 43016m 0.19 ug/L 5) EPTC 15.60 128 35605m 0.24 ug/L 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 18.49 126 52922m 0.28 ug/L 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. d 13) Terbacil 0.00 117 0 N.D. 14) Acetochlor 23.08 146 9374m 0.36 ug/L 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 24.20 162 46833m 0.07 ug/L 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 26.66 246 31075 0.15 ug/L 84 22) Bis (2-Ethylhexyl) adipate 28.90 129 15224 1.58 ug/L 89 23) Bis (2-Ethylhexyl) phthala 30.31 149 35407m 1.35 ug/L 24) Benzo (a) pyrene 33.45 252 18392m 0.79 ug/L

(#) = qualifier out of range (m) = manual integration C02A0501.D 050102.M Mon May 06 17:41:46 2002 Page 1

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Method 525.2 compound analysis results, May 2002 · Box DEP Box 65

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Analytical results for organic compounds including hexachlorobenzene and EPTC using Method 525.2 in early May 2002.

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