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Sample AD28106 Method 525.2 analysis, Jan 2002

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Laboratory results for sample AD28106 analyzing pesticides and organic contaminants using Method 525.2.

NYC-WTC_000055463–000055468

Folder label: “525 X 11/21/01 A 12/11/01 + REANALYSIS 1/25/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\012502A\28106RR.D Vial: 22 Acq On : 26 Jan 2002 6:25 am Operator: McLean Sample : REINJ Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Jan 28 12:34:41 2002 Quant Results File: 012402B.RES

Quant Method : C:\MSDCHEM\1\5973N\012402B.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Fri Jan 25 11:19:14 2002 Response via : Initial Calibration DataAcq Meth : 012402DF

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 17.96 164 11104516 5.00 ug/L 0.00 9) Phenanthrene D-10 22.28 188 16778142 5.00 ug/L 0.00 20) Chrysene D-12 30.03 240 11694012 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 12.89 134 2846789 5.00 ug/L 0.00 Spiked Amount 5.000 Recovery = 100.00% 19) Triphenyl Phosphate 29.33 326 2996797 5.93 ug/L 0.00 Spiked Amount !5.000 Recovery = 118.60% 21) Perylene D-12 34.02 264 7630963 4.60 ug/L 0.00 Spiked Amount 5.000 Recovery = 92.00%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 14.99 237 27114 0.68 ug/L 90 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 15.84 128 5038 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 18.88 126 11001 Below Cal # 1 10) Simazine 0.00 201 0 N.D. d 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 23.29 160 12012 0.16 ug/L 75 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. d 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. d 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.33 129 44163 0.53 ug/L 59 23) Bis (2-Ethylhexyl) phthala 30.69 149 274104 0.49 ug/L 94 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 28106RR.D 012402B.M Mon Jan 28 12:37:03 2002 Page 1

NYC-WTC_000055466

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NYC-WTC_000055466Source: NYC Law Department, mirrored locally

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