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Sample AD28164 Method 525.2 analysis, Jan 2002

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Laboratory results for sample AD28164 analyzing pesticides and organic contaminants using Method 525.2.

NYC-WTC_000055469–000055474

Folder label: “525 X 11/21/01 A 12/11/01 + REANALYSIS 1/25/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\012502A\28164RR.D Vial: 6 Acq On : 25 Jan 2002 6:25 pm Operator: McLean Sample : REINJ Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Jan 28 12:37:15 2002 Quant Results File: 012402B.RES

Quant Method : C:\MSDCHEM\l\5973N\012402B.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Fri Jan 25 11:19:14 2002 Response via : Initial Calibration DataAcq Meth : 012402DF

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 17.96 164 2581513 5.00 ug/L 0.00 9) Phenanthrene D-10 22.27 188 18322216 5.00 ug/L 0.00 20) Chrysene D-12 30.03 240 13159699 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 12.89 134 3580340 27.06 ug/L 0.00 Spiked Amount 5.000 Recovery = 541.20% 19) Triphenyl Phosphate 29.33 326 3149945 5.71 ug/L 0.00 Spiked Amount 5.000 Recovery = 114.20% 21) Perylene D-12 34.02 264 3249153 1.74 ug/L 0.00 Spiked Amount 5.000 Recovery 34.80%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. d 4) Hexachlorobenzene 21.13 284 6250 0.04 ug/L 64 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 18.90 126 8599 Below Cal # 1 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. d 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. d 15) Metribuzin 0.00 198 0 N.D. d 16) Metolachlor 0.00 162 0 N.D. d 17) Butachlor 26.30 160 8644 0.35 ug/L 82 18) 4,4'-DDE 27.03 246 5488 0.04 ug/L 68 22) Bis (2-Ethylhexyl) adipate 29.27 129 21799 0.51 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 30.70 149 156038 0.43 ug/L 96 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 28164RR.D 012402B.M Mon Jan 28 12:39:47 2002 Page 1

NYC-WTC_000055472

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NYC-WTC_000055472Source: NYC Law Department, mirrored locally

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