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← Document results/DEP Box 30/525 X 11/21/01 A 12/11/01 + REANALYSIS 1/25/02
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Sample AD28166 Method 525.2 analysis, Jan 2002

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Laboratory results for sample AD28166 analyzing pesticides and organic contaminants using Method 525.2.

NYC-WTC_000055475–000055480

Folder label: “525 X 11/21/01 A 12/11/01 + REANALYSIS 1/25/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

i Data File : C:\MSDCHEM\l\DATA\012502A\28166RR.D Vial: 7 Acq On : 25 Jan 2002 7:10 pm Operator: McLean Sample : REINJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Jan 28 12:40:02 2002 Quant Results File: 012402B.RES

Quant Method : C:\MSDCHEM\1\5973N\012402B.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Fri Jan 25 11:19:14 2002 Response via : Initial Calibration DataAcq Meth : 012402DF

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 17.96 164 14263485 5.00 ug/L 0.00 9) Phenanthrene D-10 22.27 188 18670009 5.00 ug/L 0.00 20) Chrysene D-12 30.03 240 13361418 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 12.89 134 3709701 5.07 ug/L 0.00 Spiked Amount 5.000 Recovery = 101.40% 19) Triphenyl Phosphate 29.33 326 3370287 5.99 ug/L 0.00 Spiked Amount 5.000 Recovery = 119.80% 21) Perylene D-12 34.02 264 7206213 3.80 ug/L 0.00 Spiked Amount 5.000 Recovery = 76.00%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. d 4) Hexachlorobenzene 21.14 284 16149 0.02 ug/L 83 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 18.70 165 72739 0.98 ug/L 27 8) Molinate 18.90 126 5657 Below Cal # 1 10) Simazine 0.00 201 0 N.D. d 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. d 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. d 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 24.59 162 6715 0.22 ug/L 81 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 27.05 246 9571 0.04 ug/L 96 22) Bis (2-Ethylhexyl) adipate 29.27 129 60671 0.53 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 30.69 149 612843 0.60 ug/L 96 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 28166RR.D 012402B.M Mon Jan 28 12:43:58 2002 Page 1

NYC-WTC_000055478

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NYC-WTC_000055478Source: NYC Law Department, mirrored locally

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