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Sample AD28105 Method 525.2 analysis, Jan 2002

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Analytical results for sample AD28105 under Method 525.2 showing compounds detected below minimum detection levels.

NYC-WTC_000055391–000055396

Folder label: “525 X 11/21/01 A 12/11/01 + REANALYSIS 1/25/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\012502A\28105RR.D Vial: 21 Acq On : 26 Jan 2002 5:40 am Operator: McLean Sample : REINJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Jan 28 12:31:48 2002 Quant Results File: 012402B.RES

Quant Method : C:\MSDCHEM\1\5973N\012402B.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Fri Jan 25 11:19:14 2002 Response via : Initial Calibration DataAcq Meth : 012402DF

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 17.96 164 13245273 5.00 ug/L 0.00 9) Phenanthrene D-10 22.27 188 18646394 5.00 ug/L 0.00 20) Chrysene D-12 30.03 240 14448651 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 12.89 134 3374059 4.97 ug/L 0.00 Spiked Amount 5.000 Recovery = 99.40% 19) Triphenyl Phosphate 29.33 326 3484003 6.20 ug/L 0.00 Spiked Amount 5.000 Recovery = 124.00% 21) Perylene D-12 34.02 264 9483383 4.62 ug/L 0.00 Spiked Amount 5.000 Recovery = 92.40%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. d 4) Hexachlorobenzene 21.14 284 6382 N.D. 5) EPTC 15.65 128 5050 Below Cal # 1 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 18.67 165 3752 0.90 ug/L 62 8) Molinate 18.89 126 7327 Below Cal # 1 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. d 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. d 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.26 129 32882 0.52 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 30.70 149 302114 0.48 ug/L 97 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 28105RR.D 012402B.M Mon Jan 28 12:32:40 2002 Page 1

NYC-WTC_000055394

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NYC-WTC_000055394Source: NYC Law Department, mirrored locally

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