Laboratory blank analysis results, sample AE11755, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File ; C:\MSDCHEM\l\DATA\051302\LBA0513.D Vial: 8 • Acq On : 13 May 2002 5:46 pm Operator: Bohlk / Inst 213 Sample : LB 5/10/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\050802.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L

Peak Number 11 Docosane, 11-decyl- (CAS) $... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

21.98 0.07 ug/L 55581 Phenanthrene d-10 22.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Docosane, 11-decyl- (CAS) $$ 11-... 451 C32H66 055401-55-3 83 2 Pentacosane $$ n-Pentacosane 352 C25H52 000629-99-2 83 3 Tricosane (CAS) $$ n-Tricosane 324 C23H48 000638-67-5 83 4 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 78 Abundance Scan 1202 (21.978 min): LBA0513.D (-) m/z 71.10 100.00% 71

5000 99 127 1A —Aa 21.6021.8022:0022:20 0- "I 4 169 ■ • j ■ l ■ ■ 1 ■ m/z 57.00 75.32% n/z-> 50 100 150 200 250 300 350 Abundance #355038: Docosane, 11-decyl- (CAS) $$ 11-n-Decyldocosane S... 57

5000 85 Mauadat.pM/M 21 60 21.80 22.00 22.20 m/z 85.10 73.84% 113 0- 44 1,4141,169197.225 250 —3450 100 *)i3 miz-> 150 ‘ ‘ 200 ' ’ 250 300 350 Abundance #300501: Pentacosane $$ n-Pentacosane 57

21.60 21.80 22.00 22.20 5000 m/z 99.10 36.51% 85

28 1 113 n/z-> 0- —44 1 141 1 169 189 21 1,239 267 295 323 50 100 1097 1* i 150 200 ।f r i 1 [ ‘i f i’| । i । 250 300 352 350 Abundance #275685: Tricosane (CAS) $$ n-Tricosane 57 21.60 21.80 22.00 22.20 m/z 113.10 27.04%

5000 85

I113 141 28 0 4-tr144414198211239267295324 ■ i ■ • ■ ■ i ■ ■ ’ f v m/z—> 50 ___ 100 150 200 250 300 350 21.60 21.80 22.00 22.20

BA0513.D 050802.M Tue May 14 10:36:15 2002 Page 13

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