GCMS surrogate recovery results, sample AE07115, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohlk Sample : SAMPLE 7115 3/27/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C;\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peale Number 10 Octadecanoic acid, 2-hydrox. . . Concentration Ranle 13

R.T. EstConc . Area Relative to ISTD R.T.

29.90 22.85 ug/L 2798000 Chrysene-dl2 30.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecanoic acid, 2-hydroxyethy ... 328 C20H40O3 000111-60-4 87 2 Undecanedioic acid (CAS) $$ 1,9-... 216 C11H20O4 001852-04-6 27 3 Tridecanedioic acid, dimethyl es... 272 C15H28O4 001472-87-3 27 4 n-Hexylamine, N-acetyl-l-cyano- 168 C9H16N2O 000000-00-0 18 flibundance Scan 4565 (29.901 min): 7115.D (-) m/z 104.05 100.00% 55 1(114

wwai

0 JMl 84

I 1^.19) 249 1 267 328 J -r-p-n-r 29.60 29.80 30.00 30.20 m/z 98.10 91.72% m/z-> 20 40 60 80 160 120 140 160 180 200 220 240 260 280 300 320 Abundance #279334: Octadecanoic acid. 2-hydroxyethyl ester $S Steari... 43 104

69 29.60 29180 30100 30.20 267 m/z 55.10 86.93%

44^Jw f 285 328

m/z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 4-.au. Abundance #138126: Undecanedioic acid (CAS) $$ 1.9-Nonanedicarboxyli...

55 73 29.60 29.80 30.00 30.20 m/z 43.10 85.73%

139

0 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #215841: Tridecanedioic acid, dimethyl ester (CAS) $$ METH... -J 98 29.60 29.80 30.00 30.20 55 74 m/z 57.10 70.43%

5000

149167

0 f ■n/z-> ;20 40 60 80 100 120 140 160 180 200 220 240 260280300320 29.60 29.80 30.00 30.20

7115.D 5080402BB.M Mon Apr 15 18:16:33 2002 Page 13

NYC-WTC_000061127