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Sample AE10187 analysis results, May 2002

Machine-extracted title · confidence 90%

Analytical results for sample AE10187 analyzed on May 6, 2002, listing compounds detected below the method detection limit.

NYC-WTC_000082581–000082617

Folder label: “525 X 4/30/02 A 5/1/02

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Scanned page image, NYC-WTC_000082615
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050202\10187.D Vial: 23 Acq On 2 May 2002 7:46 pm Operator: Bohllc / Inst 213 Sample SAMPLE 10187 4/30/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peale Number 17 5,7-Dioxooctanoic acid, met... Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T.

26.50 0.05 ug/L 126160 p-Terphenyl d-14 26.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 5,7-Dioxooctanoic acid, methyl e... 186 C9H14O4 000000-00-0 38 2 (7-2H3)PIPERITONE $$ 2-Cyclohexe... 155 C10H13D3O 054193-88-3 30 3 7-Tridecanone 198 C13H26O 000462-18-0 22 4 3,6-Dimethyl-2,4-heptadione 156 C9H16O2 000000-00-0 22 Abundance Scan 1700 (26.495 min); 10187.D (-) m/z 57710 100.00% 57

85

113 5000

141 . 178198 352 26.20 26.40 26.60 26.80

'n/z-> 0 1 50 1 t jjJjIi .hiiljllillli I 100 150 200 250 300 I I 350 m/z 85.10 70.41%

Abundance #94855; 5,7-Dioxooctanoic acid, methyl ester 43 85 113

5000 26.20 26.40 26.60 26.80 m/z 113.10 50.85% 186 0 luL 1 J I -n/z-> 50 100 150 200 250 300 350 Abundance #50426: (7-2H3)PIPERITONE SS 2-Cyclohexen-1-one, 3-(melhyl... 85 113 26.20 26.40 26.60 26.80 Wilill “m/z 69.10 49.86%

41 140 I 0 65 I nn/z-> 50 100 150 200 250 300 350 Abundance #113087: 7-Tridecanone 43 26.20 26.40 26.60 26.80 113 m/z 71.10 41.07%

5000 85

m/z-> 0 jUM 50 100 T ,169 150 200 250 300 350 26.20 26.40 26.60 26.80

10187.D 050102.M Mon May 06 15:08:17 2002 Page 19

NYC-WTC_000082615

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NYC-WTC_000082615Source: NYC Law Department, mirrored locally

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