Sample AE10187 analysis results, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050202\10187.D Vial: 23 Acq On 2 May 2002 7:46 pm Operator: Bohlk / Inst 213 Sample SAMPLE 10187 4/30/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P,

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L *********★****★★***★***★****■*★**********★★★*★*★★**★★■*★■*****★***★★★★★*

Peale Number 16 (E)-2,4'-dihydroxystilbene ... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. JL-vo 25.98 3.59 ug/L 8367050 p-Terphenyl d-14 26.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 (E)-2,4'-dihydroxystilbene $$ 2,... 212 C14H12O2 110983-43-2 72 2 [2.2)(2,6)pyrazinophane :212 C12H12N4 123624-86-2 64 3 [1,1'-Biphenyl)-4,4'-diamine, 3,... :212 C14H16N2 000119-93-7 59 4 Benzenamine, 2-methoxy-N-(4-pyri... :212 C13H12N2O 041855-68-9 53 Abundance Scan 1643 (25.978 min): 10187.D (-) m/z 212.20 100.00% 2 2

I 5000

106 ■p*

Ti/z-> Abundance 20 1^ y. I'll,, 40__ 60 80 100 120 140 160 180 200 220 240 260 180104 238 261 4, ' ' I ' ' ' ' I• 25.60 25.80 26.00 26.20 m/z 106.10 18.68%

#133665: (E)-2,4'-dihydroxystilbene S$ 2,4'-Dihydroxy-stiL.. 2 2

5000 I ‘ ' I 25.60 25.80 26.00 26.20 m/z 211.20 18.14% 118 I T Tr til III, I. Lt ,11 ■fVi l“|•| i"|‘, I i"l“p •n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #132924: [2.2](2,6)pyrazinophane 2 2

25.60 25.80 26.00 26.20 5000 m/z 213.20 16.30%

158 185 1^ l 0 I. ■.. I • I ' ' ' ' I Tl/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #133757: [1,r-Biphenyl]-4,4'-diamine, 3,3'-dimethyl- 2 2 25.60 25.80 26.00 26.20 m/z 208.20 16.19%

Wilil I ? 51 77 91J130 152166^^ T 0 ' I'' '' I ' '' ' I' ' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 25.60 25.80 26.00 26.20

10187.D 050102.M Mon May 06 15:08:16 2002 Page 18

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