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Reference standard analysis results, sample AE10186, May 2002

Machine-extracted title · confidence 90%

Results for reference standards including hexachlorobenzene and alachlor analyzed between April 30 and May 2, 2002.

NYC-WTC_000082548–000082580

Folder label: “525 X 4/30/02 A 5/1/02

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Scanned page image, NYC-WTC_000082577
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050202\10186.D Vial: 22 Acq On 2 May 2002 6:59 pm Operator: Bohlk / Inst 213 Sample SAMPLE 10186 4/30/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Pealt Number 13 Pyrene, 2-methyl- (CAS) $$ ... Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

25.79 0.06 ug/L 153714 p-Terphenyl d-14 26.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pyrene, 2-methyl- (CAS) $$ 2-Met... 216 C17H12 003442-78-2 50 2 Pyrene, 4-methyl- $$ 4-Methylpyrene 216 C17H12 003353-12-6 47 3 Bicyclo[3.3.1]nonan-9-ol, 1-phen... 216 C15H20O 036399-43-6 43 4 .ALPHA.,.ALPHA.'-DIFLUOROSTILBEN... 216 C14H10F2 000643-76-5 43 Abundance Scan 1622 (25.788 min): 10186.D (-) m/z 216.05 100.00% 2 6

108 55 70 84 170 I ' '' ’ I ' ' I ' 25.40 25.60 25.80 26.00 26.20 I, I ,b|, ,121 136^'*® 191 236 m/z 215.20 32.79% 0 m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #139295: Pyrene, 2-methyl- (CAS) S$ 2-Methylpyrene 2 6

5000 25.40 25.60 25.80 26.00 26.20 m/z 217.20 23.45% 95 infl I 108 189 I 51, . 81, ,1,1^ I 135 150163176 . 0 m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #139297: Pyrene, 4-methyl- $$ 4-Methyipyrene 2 6

.. |l...l,w.l..... 25.40 25.60 25.80 26.00 26.20 m/z 108.25 23.04%

??■ r. IT? 189 ',i^ Vr-rrn-T-r

luuUita Oi ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #139085: Bicyclo[3.3.1]nonan-9-ol, 1-phenyl- $$ 1-Phenylbi... 2 6 25.40 25.60 25.80 26.00 26.20 m/z 107.90 18.52% 91 157

5000 118 I 130 198 40 105 77

idJWli 170 185 0 . ill II h ilL . t J , . I '.I' . 1 I ' ' ' ' I ' ' ' ' I ' Tl/z-> 40 60 80 100I 120 140 160 180 200 220 240 25.40 25.60 25.80 26.00 26.20 |

10186.D 050102.M Mon May 06 14:53:55 2002 Page 15

NYC-WTC_000082577

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NYC-WTC_000082577Source: NYC Law Department, mirrored locally

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