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Reference standard analysis results, sample AE10186, May 2002

Machine-extracted title · confidence 90%

Results for reference standards including hexachlorobenzene and alachlor analyzed between April 30 and May 2, 2002.

NYC-WTC_000082548–000082580

Folder label: “525 X 4/30/02 A 5/1/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050202\10186.D Vial: 22 Acq On 2 May .2002 6:59 pm Operator: Bohllc / Inst 213 Sample SAMPLE 10186 4/30/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 14 [2.2](2,6)pyrazinophane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.98 3.44 ug/L 8772330 p-Terphenyl d-14 26.77 AMP Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 [2.2](2,6)pyrazinophane 212 C12H12N4 123624-86-2 59 2 [1,1'-Biphenyl]-4,4' -diamine, 3, . . . 212 C14H16N2 000119-93-7 59 3 [1,1'-Biphenyl]-4,4'-diamine, 3, . . . 212 C14H16N2 000119-93-7 59 4 [1,1'-Biphenyl]-4,4'-diamine. 3, . . . 212 C14H16N2 000119-93-7 59 Abundance Scan 1643 (25.979 min): 10186.D (-) m/z 212.20 100.00% 2 2

5000

106 25.60 25.80 26.00 26.20 194 149156 180iq4256 m/z 106.10 19.22% 0 TT-pr-n-r-p- ' I''' * I'''' I'''' I'' m/z-> :20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #132924: [2.2](2,6)pyrazinophane 2 2

5000 25.60 25.80 26.00 26.20 185 m/z 211.20 17.50% 158

ni/z-> 0 ,.... 11 20 40 60 80 I'''' I XU .1^ 100 120 140 160 180 200 220 240 260 Abundance #133759; [1,1'-BiphenylJ-4,4-diamine. 3,3'-dimelhyl- S$ B... 2 2

25.60 25.80 26.00 26.20 m/z 213.20 16.82% 5000

28 , | , n . I'l, I .‘'7° ,!■. I...... . . 0 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #133757; [1,1'-Biphenyt]-4,4'-diamine, 3,3'-dimethyl- pTTryr I 1111 2 2 25.60 25.80 26.00 26.20 m/z 208.10 16.39%

5000

28 106 iftn 19® 130 152167y|° 0 l-m-r ■p" r^-'' I' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 25.60 25.80 26.00 26.20

10186.D 050102.M Mon May 06 14:53:56 2002 Page 16

NYC-WTC_000082578

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NYC-WTC_000082578Source: NYC Law Department, mirrored locally

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