Sample AE10187 analysis results, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050202\10187.D Vial: 23 Acq On 2 May 2002 7:46 pm Operator: Bohlk / Inst 213 Sample SAMPLE 10187 4/30/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peale Number 14 1,2-Benzenedicarboxylic aci... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

24.06 0.20 ug/L 450140 Phenanthrene d-10 21.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, di. . . 334 C20H30O4 000084-75-3 59 2 Dibutyl phthalate 278 C16H22O4 000084-74-2 53 3 1,2-Benzenedicarboxylic acid, bu... 334 C20H30O4 000084-78-6 53 4 1,2-Benzenedicarboxylic acid. di. . . 306 C18H26O4 000131-18-0 53 Abundance Scan 1432 (24.065 min); 10187.D (-) m/z 149.10 100.00% 149

5000

71 23.80 24.00 24.20 24.40 169 205223 262 m/z 71.05 15.77% 0 r| n..pI f. 11 J '^^1 n/z-> 20 40 60 80 100120140160180200220240260280300 320 Abundance #284881; 1,2-Benzenedicarboxylic acid, dihexyl ester 1 ■9

Sia ' ' ' p' ' ' I ' ' ' ' 23.80 24.00 24.20 24.40 43 m/z 57.05 14.26%

167 203 233^51 278 334 0 I" " I" " I" " I" ' I"'' I" " I' ‘ m/z-> 20 40 60 80 100120140160180200220240260280 300320 *\bundance #223232; Dibutyl phthalate 149

23.80 24.00 24.20 24.40 5000 m/z 85.10 10.66%

0 il, . I r r. .195123 i I |H . . I h. . f. . I >1 |m . 11... I... 11 H . ■n/z-> 20 40 60 80 100120140160180200220240260280 300320 ^^bundance #284877; 1,2-Benzenedicarboxylic acid, butyl octyl ester $... 1 .9 23.80 24.00 24.20 24.40 m/z 150.00 8.45%

41 167 205^23 261279 334 0 I 11 I I I I ... I I I I . |1 I I I j I . I . (H. .1 I I 1''" I' m/z-> 20 40 60 80 100120140 160180 200 220 240 260 280 300 320 2X8()24'()() 24.2024'40

L0187.D 050102.M Mon May 06 15:08:13 2002 Page 16

NYC-WTC_000082607