NYC-WTC_000051122
Laboratory report showing GCMS analysis of sample AE00319 for unknown compounds and DDD on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗Document / 14 pages
GCMS reference standard results for sample AE00327, Jan 2002
Machine-extracted title · confidence 100%Laboratory report showing GCMS analysis of reference standards used for calibration during January 10-11, 2002 testing.
NYC-WTC_000051165–000051178Folder label: “GCMS X 1/8/02 A 1/10/02”
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OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\5973N\02JAN10\0108R.D Vial: 2 Acq On : 10 Jan 2002 1:11 pm Operator: Sample : ref ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSC.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 1,2-Benzenedicarboxylic aci... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.
21.72 0.11 ug/L 65529 Phenanthrene-dl 0 22.65
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,2-Benzenedicarboxylic acid, bu... 236 C13H1604 034006-76-3 83 2 l-Methoxy-2-tert-butyl-6-methylb... 178 C12H180 060772-80-7 74 3 METHYL 2-ETHYLHEXYL PHTHALATE $$... 292 C17H24O4 000000-00-0 64 4 1,2-Benzenedicarboxylic acid, bu... 236 C13H1604 034006-76-3 64 Abundance Scan 1607 (21.721 min): 0108R.D (-) m/z 163.00 100.00% 163 J 149
5000
77 ■ ■ ' I 181 21.40 21.60 21.80 22.00 50 65 . 92 105 133 39 II/Balyish, 0- ■ ■ i ■ H m/Z 149.00 74.55% m/z-> 40 60 80 100 120 160140 180 200 220 240 Abundance #167333:1,2-Benzenedicarboxylic acid, butyl methyl ester... 1$3 149 ......... . ........... 5000 21.40 21.60 21.80 22.00 m/z 77.00 18.81%
m/z-> 77 92 104 121 135 0 ................. II,,, I., I,. TI ■ il, ■ I, ■ i 40 60 80 100 120 140 160 180 L 181 208 236 t ■ । i ■ 1 1 r• < < > । 200 220 240 Abundance #83998: 1-Methoxy-2-tert-butyl-6-methylbenzene $$ Benzene,... 149 163
178 21.40 21.60 21.80 22.00 5000 m/z 181.00 12.27%
01 ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ 1 i ■ ■ ■ ■ i 1 ■ ■ ■ I ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #240421: METHYL 2-ETHYLHEXYL PHTHALATE $$ MEHP ' i ' ' ' ' I 163 21.40 21.60 21.80 22.00 149 m/z92.00 10.59% 70 5000 181
54 83
m/z-> 0.....i ■ 40 60 - ' 135 80 II, ' 100 112
120 140 'i 160 180 200 220 240 .II..... 21.40 21.60 21.80 22.00
0108R.D W042302.M Thu May 02 14:37:27 2002 Page 4
NYC-WTC_000051173
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NYC-WTC_000051173Source: NYC Law Department, mirrored locally
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NYC-WTC_000004935
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