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Document / 14 pages

GCMS reference standard results for sample AE00327, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of reference standards used for calibration during January 10-11, 2002 testing.

NYC-WTC_000051165–000051178

Folder label: “GCMS X 1/8/02 A 1/10/02

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Scanned page image, NYC-WTC_000051174
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN10\0108R.D Vial: 2 Acq On : 10 Jan 2002 1:11 pm Operator: Sample : ref ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSC.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 2 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.14 ug/L 81092 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 59 3 Myristicine 192 C11H1203 000000-00-0 52 4 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 42 Abundance Scan 1656 (22.280 min): 0108R.D (-) m/z 192.10 100.00% 192

5000 ............ ,............... ,, 82 96 146 160

n/z-> 0 64 44 TPPPT T‘‘T 1 T 118 | < .'I'. | < I ■ ■ | ■ 1 I I | ■ ■ । I'f lTr

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 4 22.00 22.20 22.40 22.60 m/z 191.10 16.58% Abundance #102588:4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 TTI 22.00 22.20 22.40 22.60 146 175 m/ Z 193.10 i 14.75%

0 TII 1’21719000 I ■''' I T‘ ............I1 Tap m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192

22.00 22.20 22.40 22.60 5000 82 m/z96.00 14.09%

54 110 30 94 0 ""I............ "I'"....... 160 " i " " r " ' r ' " r ' " I" " i " " i " '1 TT mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102653: Myristicine 192 22.00 22.20 22.40 22.60 m/z 146.10 13.43% 5000

91 119 131 165 65 77 "I... ... 1. 1, .. 1 . ‘I‘ 93 . . . । ... . । n ‘‘I11 147 | 0 > . ‘ I’’ I \ I''1' 11''' I'''' I' " ' I m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

0108R.D W042302 .M Thu May 02 14:37:28 2002 Page 5

NYC-WTC_000051174

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NYC-WTC_000051174Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.989

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.988

machine-extracted · confidence unavailable · Check page ↗

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