GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\30648A.D Vial: 5 Acq On 5 Feb 2002 2 : 03 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 22.28 0.17 ug/L 207156 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 64 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 53 3 9H-Fluorene, 9-ethylidene- (CAS) 192 C15H12 007151-64-6 53 4 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 Abundance Scan 1656 (22.280 min): 30648A. D (-) m/z 192.10 100.00% 19/2

5000 -

82 96 146 160 40 54 66 | J 118 22.00 22.20 22.40 22.60 0 TTTTNHHmhttmmu "I"'1!"" I" "l‘11 000..... ........ Wp m/z 191.10 17.30% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588:4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

5000' 108 ..... y.... A 22.00 22.20 22.40 22.60 146 175 m/ z 96.10 15.09%

m/z—> 0'' i'" ' i " " i ■ ■ " i" 1' i' " ' r 1" i " " i " i1" ■ 1111' i" " i" ■ i ■ " ' i ■ •" i ■ ......... 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 U Abundance #88409: N-perdeuteriobenzylideneaniline 192

22.00 22.20 22.40 22.60 5000' 82 m/z 146.10 14.51%

54 110 0 m 30 ■' r "' i" 1 mHH 94 160 — I “ " 11 *' * 11'111 /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 4 Abundance #103905:9H-Fluorene, 9-ethylidene- (CAS) 192 Asm 22.00 22.20 22.40 22.60 m/z 193.10 14.09%

5000 165

83 99

0 .... 45........... | " i"'1111" i"11111 ‘11 ■' ■ • ।''11111'' । I’111" " i1111 tgn z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

30648A.D SCAN508.M Thu Feb 21 10:19:05 2002 Page 13

NYC-WTC_000004930

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