Laboratory report for sample AE00103 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
NYC-WTC_000050384–000050396Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN23\00103.D Vial: 5 Acq On : 23 Jan 2002 6:15 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 78433 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 3 fluorene-9-spiro-cyclopropane 192 C15H12 000000-00-0 45 4 1,5-Naphthalenedithiole 192 C10H8S2 000000-00-0 45 Abundance Scan 1656 (22.280 min): 00103. D (-) m/z 192.10 100.00% 192
5000- ...... ...... 96 146 160 82 118 22.00 22.20 22.40 22.60 0 mmmmml ‘I ।... I। । t T i““t m/z 191.10 17.50% miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140150 160 170 180 190 200 Abundance #102588:4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192
108 5000 22.00 22.20 22.40 22.60 146 175 m/z 96.00 16.46%
m/z—> U 0 ... ।.... ।,... ।. 11. i।. i. ।. j. . I. । ... I''' ■ I'''' I'' ‘' I' ‘ ' I''' ‘ 1' ‘ " I ‘ H 20 30 40 50 60 70 80 90 100 110 120 130 140150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192 - 22.00 22.20 22.40 22.60 5000 82 m/z 146.10 16.01% 54 110 94 O mtrreryreT* 30 160 nyllijn —MT 11111 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103959: fluorene-9-spiro-cyclopropane ........... A 1—1** ■ ‘ I ‘ ‘ ' I ' ' ‘ ‘ 1 ‘ 192 22.00 22.20 22.40 22.60 m/z 193.10 12.93% 165 5000-
miz--> 0 7 U 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 — 22.00 22.20 22.40 22.60
00103.D SCAN508.M Thu Jan 24 09:57:19 2002 Page 7
NYC-WTC_000050394
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000050397
Laboratory report for sample AE00698 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050024
Laboratory report showing GCMS analysis of sample AD31671 including unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050370
Laboratory report for sample AE00101 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051380
Laboratory report showing GCMS analysis of sample AE00315 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050334
Laboratory report for sample AD31677 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051471
Laboratory report showing GCMS analysis of sample AE00469 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049902
Laboratory report showing GCMS analysis of sample AD31585 including unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050205
Laboratory report documenting GCMS analysis of sample AD31647 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049916
Laboratory report showing GCMS analysis of sample AD31631 including unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050411
Laboratory report for sample AE00838 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049944
Laboratory report showing GCMS analysis of sample AD31638 including unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050258
Laboratory report documenting GCMS analysis of sample AD31664 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000050177
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050178
Instrument log sheet recording sample counts and operational parameters for GCMS Method 508 analysis in January 2002.
Filed in the same folder
NYC-WTC_000050180
Calibration report for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050184
Reference scan data for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050189
Blank analysis report for GCMS testing of sample AD31647 confirming no contamination above detection limits.
Filed in the same folder