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GCMS analysis results for sample AE00840, Feb 4 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00840 including surrogate recovery and unknown compounds.

NYC-WTC_000052108–000052127

Folder label: “GCMS X 1/11/02 A 1/31/02

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Scanned page image, NYC-WTC_000052124
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File : C: \MSDCHEM\1\5973N\02JAN31\00840.D Vial: 4 Acq On : 31 Jan 2002 5:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L *************************************************************** ** **** Peak Number 11 4-METHOXY-.BETA.-METHYLCINN. .. Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.16 ug/L 124660 Phenant hrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 fluorene-9-spiro-cyclopropane 192 C15H12 000000-00-0 59 3 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 59 4 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 Abundance Scan 1656 (22.280 min): 00840. D (-) m/z 192.10 100.00% 192

5000

82 96 146 160 22.00 22.20 22.40 22.60 42 52 66 I I 120 | 0 NITT Mi '^T1' 11 < 111 n-H 111 < 11 > 111 111 > 111 111111 1111111 111 hi । !■.. I> . । TT‘ m/z 191.10 17.92% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588: 4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 TU 22.00 22.20 22.40 22.60 146 175 m/z 193.10 15.54%

0 TT ITTTT’ I I I | I I M | I I I . | | | I' " ' I' ‘ ' I''1' I 'I '| UM |' L m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103959: fluorene-9-spiro-cyclopropane 192 • ■ । 1 » > । । ■ ■ > • । ‘ ' 165 22.00 22.20 22.40 22.60 5000 m/z 146.10 14.11%

87 96 rn/z—> 0 " i " " i" " i" " i" " i " " i'"" i' 139 i ' r '1 r i' " ■ i' ■ " i ■ " 11 ■ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 1752... L Abundance #88409: N-perdeuteriobenzylideneaniline Tur .A i ‘ ■ 1 192 22.00 22.20 22.40 22.60 m/z96.10 12.32%

5000 82

54 110 30 1 94 160 0 -TPTTTT 1 ■ i1"11" —H " i■ ■■ ■ i''"i"■'i"I"‘'i — TIT" ..................... ..... , m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

00840.D SCAN508.M Fri Feb 01 09:19:22 2002 Page 13

NYC-WTC_000052124

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NYC-WTC_000052124Source: NYC Law Department, mirrored locally

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