GCMS analysis results, sample AE02718, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\5973N\02FEB28\02718.D Vial: 3 Acq On : 28 Feb 2002 4:20 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 1,2-Benzenedicarboxylic aci... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

24.86 0.11 ug/L 69414 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, bi... 282 C14H1806 000117-82-8 83 2 1,2-Benzenedicarboxylic acid, di... 278 C16H2204 000084-74-2 83 3 Dibutyl phthalate 278 C16H2204 000084-74-2 83 4 Dibutyl phthalate 278 C16H2204 000084-74-2 83 Abundance Scan 1903 (24.857 min): 02718.D (-) m/z 149.00 100.00% 149

5000

41 57 76 105 121 205 223 24.60 24.80 25.00 25.20 0 unidadiy* 11+1110—11101 f l m/z 41.10 8.08% m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #227809:1,2-Benzenedicarboxylicacld, bis(2-methoxyethy)... 149

5000 24.60 24.80 25.00 25.20 m/z 150.00 7.23% 41 56 76 0 --TH— 104 121 | .............. ... N /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223248:1,2-Benzenedicarboxylic acid, dibutyl ester (CAS)... 149

24.60 24.80 25.00 25.20 5000 m/z 223.00 5.24%

41 56 76 104 । 205 223 O'- 111 ■ ■ ■ I • • • ■ i ■ ■ • ■ i ■ ■ ■ • i ■■ ■11 ■ ' ■' i ■ • ■ ■ i11 ■ ■ i ‘ ‘ m/z—> 20 40 60 80 100 120 140 160 180 20Q 220 240 260 280 Abundance #223232: Dibutyl phthalate ■ * । 1 * > < i < ■ ■ i ■ ■ ■ ■ i ■ • 149 24.60 24.80 25.00 25.20 m/z 57.10 4.69%

5000

29 41 57 76 104 121 163 178 205 223 0 miz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 24.60 24.80 25.00 25.20

02718.D HP022102.M Fri Mar 01 10:07:29 2002 Page 15

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