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GCMS analysis results, sample AE02718, March 2002

Machine-extracted title · confidence 70%

Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.

NYC-WTC_000010967–000010986

Folder label: “GCMS X 2/5/02 A 2/28/02

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NYC 9/11 Public Portal Document Tentatively Identified Compound (LSC) summary Operator ID: Date Acquired: 28 Feb 2002 4:20 pm Data File: C:\MSDCHEM\1\5973N\02FEB28\02718.D Name: 508 scan Mise: February 28, 2002 Method: C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title: 508 scan method Library Searched: C:\DATABASE\WILEY7N.L

--Internal Standard-- TIC Top Hit name RT EstConc Units Response # RT Resp Cone Butanoic acid/ me.. 3.62 0.1 ug/L 55421 1 9.72 7695780 20.0 Propane, 1,1-dime . . 3.93 0.1 ug/L 31835 1 9.72 7695780 20.0 4-0-Methyl- .-arab. . 4.25 0.2 ug/L 62658 1 9.72 7695780 20.0 1,3,5-CYcl eptat.. 4.38 0.1 ug/L 22285 1 9.72 7695780 20.0 Butanoic abid, 2-.. 4.64 0.1 ug/L 22267 1 9.72 7695780 20.0 Cyclopentanone 4.88 0.1 ug/L 30173 1 9.72 7695780 20.0 Butenol,/ methyl- 5.02 0.1 ug/L 25247 1 9.72 7695780 20.0 3 - (CYCLOHEX-3 ‘ -EN. . . 5.94 0.3 ug/L 119908 1 9.72 7695780 20.0 Diacetamide $$ Ac . . . 6.09 0.1 ug/L 38674 1 9.72 7695780 20.0 Pyrimidinetetrami . . . 16.55 0.0 ug/L 20957 3 18.34 12089100 20.0 4 -METHOXY- . BETA - . . . 22.28 0.1 ug/L 70950 4 22.63 12786900 20.0 Phenanthrene-dl0 22.77 0.4 ug/L 278511 4 22.63 12786900 20.0 1,2-Benzenedicarp... 24.86 0.1 ug/L 69414 4 22.63 12786900 20.0

02718.D HP022102.M Fri Mar 01 10:07:29 2002 Page 16

NYC-WTC_000010986

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NYC-WTC_000010986Source: NYC Law Department, mirrored locally

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