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GCMS analysis results, sample AE02719, March 2002

Machine-extracted title · confidence 68%

Gas chromatography-mass spectrometry analysis of sample AE02719 performed March 5, 2002, reporting other unknown compounds and surrogate 2,4-DDD recovery data.

NYC-WTC_000010987–000011006

Folder label: “GCMS X 2/5/02 A 2/28/02

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NYC 9/11 Public Portal Document

Tentatively Identified Compound (LSC) summary Operator ID: Date Acquired: 28 Feb 2002 5:10 pm Data File: C:\MSDCHEM\1\5973N\02FEB28\02719.D Name: 508 scan Mise: February 28, 2002 Method: C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title: 508 scan method Library Searched: C:\DATABASE\WILEY7N.L

--Internal Standard-- TIC Top Hit name RT EstConc Units Response # RT Resp Cone Butanoic acid, me... 3.62 0.2 ug/L 53835 1 9.72 7075870 20.0 Propane , 1,1 -dime . . . 3.93 0.1 ug/L 28523 1 9.72 7075870 20.0 2-Oxetanone, ^me... 3.99 0.1 ug/L 23915 1 9.72 7075870 20.0 2-Propenenitrile, . . . 4.25 0.1 ug/L 36073 1 9.72 7075870 20.0 1,3,5 -Cycloheptat . . . 4.38 0.0 ug/L 15485 1 9.72 7075870 20.0 2,3,4,5-Tetrahydr . . . 4.90 0.0 ug/L 14499 1 9.72 7075870 20.0 Acetic acid, 3- [1... 5.94 0.4 ug/L 138801 1 9.72 7075870 20.0 DEUTEROACETONE 9.89 0.0 ug/L 13348 1 9.72 7075870 20.0 4 (1H) -Pyrimidinon. . . 13.38 0.1 ug/L 33466 2 13.20 10150600 20.0 Methylpbloroglucinol 16.55 0.0 ug/L 16104 3 18.33 10936700 20.0 N-perdeuteriobenz . . . 22.28 0.1 ug/L 58931 4 22.63 11730500 20.0 Benzenamine , N- N. . . 23.23 0.0 ug/L 14155 4 22.63 11730500 20.0 1,2-Benzenedicarb.. . 24.86 0.1 ug/L 46894 4 22.63 11730500 20.0

.02719.D HP022102.M Fri Mar 01 10:07:35 2002 Page 16

NYC-WTC_000011006

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NYC-WTC_000011006Source: NYC Law Department, mirrored locally

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