GCMS analysis results, sample AE02719, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB28\02719 .D Vial: 4 Acq On : 28 Feb 2002 5:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 1,2-Benzenedicarboxylic aci... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

24.86 0.08 ug/L 46894 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, bu... 334 C20H30O4 000085-69-8 64 2 O-DIMETHYLAMINOBENZALDEHYDE $$ B. . . 149 C9H11NO 000579-72-6 59 3 1,2-Benzenedicarboxylic acid, bi... 282 C14H1806 000117-82-8 43 4 Dibutyl phthalate 278 C16H2204 000084-74-2 43 Abundance Scan 1903 (24.857 min): 02719.D (-) m/z 149.00 100.00% 149

5000 ----- 41 57 104 205 24.60 24.80 25.00 25.20 0 ----- ■ • । t ‘ । ■1 ■ ■ i ’ • ■ • i ■ ■ ■ ■ । • • ■' । • i ■ ■ ■ • i • ■ ‘11 •' m/z 150.00 7.38% mfz~> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #284878:1,2-Benzenedicarboxylic acid, butyl 2-ethylhexyl... 149

5000- 24.60 24.80 25.00 25.20 m/ z 41.10 6.14% 0------ 56 76 104 121 1.2952.......... 27& niz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #45220:0-DIMETHYLAMINOBENZALDEHYDE $$ Benzaldehyde, 2-(di... 149 11 "11 I"’’* I 1 1 1 11 1 ' 1 ' i 44 120 24.60 24.80 25.00 25.20 77 106 5000 132 m/z 104.10 5.95% 91

1 1 । i — i — J i — rri t ] i n — n n 1 n n — r oW 1 1 i ■ ■ 111 TIIr 111 vfz~> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #227809:1,2-Benzenedicarboxyiicacid, bis(2-methoxyethy!)... 149 24.60 24.80 25.00 25.20 m/ z 49.10 5.40%

5000 / N 1 AA 41 56 76 104 121 205 223 282 0 1 1 i| ■ I T*' ‘ gi 1 ’11 "r1 1 P Is * i * ‘ ■ i1 ■ 1 * I 1 / ’Bit ’tt m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 24.60 24.80 25.00 25.20

02719.D HP022102.M Fri Mar 01 10:07:35 2002 Page 15

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