DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\02455.D Vial: 6 Acq On : 27 Feb 2002 7:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak. Number 9 1,2-Benzenedicarboxylic aci... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T. 24.86 0.08 ug/L 69606 Phenanthrene-dl0 22.64

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, bu. . . 304 C18H24O4 000084-64-0 83 2 1,2-Benzenedicarboxylic acid, bu. . . 334 C20H30O4 000085-69-8 83 3 Dibutyl phthalate 278 C16H22O4 000084-74-2 83 4 1,2-Benzenedicarboxylic acid, bu. . . 334 C20H30O4 000084-78-6 78 Abundance Scan 1903 (24.856 min): 02455.D (-) m/z 149.00 100.00% 149 A

5000 ................. ........... .................

41 56 76 104 122 205 223 24.60 24.80 25.00 25.20 0+P------------- m/ z 41.10 9.37% nz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #254298:1,2-Benzenedicarboxylic acid, butyl cyclohexyl es... 149

. A . w, 5000 ■ I'1 ■11 ■ U ■ । ■ ■ i । ■ 24.60 24.80 25.00 25.20 m/Z 150.00 8.63% 55 76 104 121 167 205 223 0+—ha h”udi“uvi " 1 1 1 I ' i . 1 I .... I 'l ... I , I .... I I ... I .... 1 .... I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #284879:1,2-Benzenedicarboxylic acid, butyl 2-ethylhexyl ... 149 * i-1 ■ ■ ■ ■ । * 24.60 24.80 25.00 25.20 5000 m/z 56.10 5.17%

A 57 76 104 121 1 205 223 261 279 334 O-TT -----— TImIP]PT ■ i ■ ■1' i 1'1 1 i1''' i1 1'' i1 1' ■ i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #223236: Dibutyl phthalate .... I ■ ■ i - ■ ■ ■ i ■ 1 1 I ‘ ■ 1 1 ' 149 24.60 24.80 25.00 25.20 m/ Z 205.00 5.07%

5000

57 76 105121 205 223 O-7 L ' ''I ■ ■11'' ■' i.... .. 11r 11 P 11*1ss1*’278 **III**p***’/’| m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 24.60 24.80 25.00 25.20

32455.D HP022102.M Thu Feb 28 08:47:43 2002 Page 11

NYC-WTC_000005120

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NYC-WTC_000005120Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999