DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\5973N\02FEB27\02455.D Vial: 6 Acq On : 27 Feb 2002 7:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Hexadecanoic acid (CAS) $$ ... Concentration Rank. 6

R.T. EstConc Area Relative to ISTD R.T.

24.72 0.15 ug/L 129231 Phenanthrene-dl0 22.64

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecanoic acid (CAS) $$ Palmi ... 256 C16H3202 000057-10-3 95 2 Hexadecanoic acid (CAS) $$ Palmi... 256 C16H3202 000057-10-3 91 3 Hexadecanoic acid (CAS) $$ Palmi... 256 C16H3202 000057-10-3 87 4 Pentadecanoic acid (CAS) $$ Pent... 242 C15H30O2 001002-84-2 83 Abundance Scan 1891 (24.721 min): 02455.D (-) m/ z 73.00 100.00% 60 73 43

5000 129 85 97 111 157 171 185 213 256 . 34 . ...... —— 24.40 24.60 24.80 25.00 I............... _ I n/z-> 0- 40 60 [III . Ill I 1 i 11 ' ’I 1 ' 1 1 i 1 ' 1 1 i ' 1 80 100 120 140 160 X ‘ 1 1 ‘ 1 ' 1 1 1 1 180 200 220 240 260 m/ Z 60.00 95.64% Abundance #195443: Hexadecanoic acid (CAS) $$ Palmitic acid $$ Palmi... 73 60 .... ......................... 5000 ■ ■ i > ■ ■ ■ । 129 24.40 24.60 24.80 25.00 85 97 213 m/ Z 43.10 78.54% 115 0 ■ ■ । 11 ... I .143/1, 1 ' 1 1 1 1 . 157 171 185 199 TTI - ■ i ■1 ■ ■ ■ । 226 256 ■ I । ■

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195433: Hexadecanoic acid (CAS) $$ Palmitic acid $$ Palmi... 43 73 , WWW AMA A 60 ■ ■ i ' ■ ■ ■ i ' 1 1 1 I 1 ■ ' 1 i ’ 1 1 1 t 87 24.40 24.60 24.80 25.00 5000 m/ z 57.10 69.55% 129 i 98 143 185 213 227 256 O-TT , .. I , III. i I, I — mz-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195442: Hexadecanoic acid (CAS) $$ Palmitic acid $$ Palmi... 43 60 73 24.40 24.60 24.80 25.00 m/z 55.10 66.78%

5000

85 97 129 213 0 | 111 157 171 185 I 1228 — 256 AAN....... m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 24.40 24.60 24.80 25.00

22455.D HP022102.M Thu Feb 28 08:47:43 2002 Page 10

NYC-WTC_000005119