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GCMS analysis results for sample AE06853, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE06853 conducted on April 11, 2002, identifying unknown compounds.

NYC-WTC_000060649–000060663

Folder label: “GCMS X 3/22/02 A 4/7/02

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Scanned page image, NYC-WTC_000060656
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\040502\6853.D Vial: 46 * Acq On .7 Apr 2002 8:44 am Operator: Bohl)c Sample SAMPLE 6853 3/22/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\MSDCHEM\l\5973N\5080402.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Hexadecanoic acid (CAS) $$ ... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

24.62 0.40 ug/L 229204 Phenanthrene-dl0 22.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecanoic acid (CAS) $$ Palmi... 256 C16H32O2 000057-10-3 96 2 n-Hexadecanoic acid 256 C16H32O2 000057-10-3 95 3 Hexadecanoic acid (CAS) $$ Palmi... 256 C16H32O2 000057-10-3 94 4 Hexadecanoic acid (CAS) $$Palmi... 256 C16H32O2 000057-10-3 93 Abundance Scan 3666 (24.619 min): 6853.D (-) m/z 73.10 100.00% 6(0 7l3

43 5000 129

m/z-> OV 20 40 J, Wi 60 80 115 143 171185 213

100 120 140 160 180 200 220 240 260 /Abundance . #195439: Hexadecanoic acid (CAS) S$ Palmitic add $S Palmi... X 256 24.20 24.40 24.60 24.80 25.00 m/z 60.10 99.58%

43 60 73

5000 ........ ... 24.20 24.40 24.60 24.80 25.00 m/z 57.10 83.92% i7 129

Ti/z-> OV 20 I.60 80 100 120p ,1. 140 160 180 200 J?,220......240 260 40 Abundance ' #195431; n-Hexadecanoic acid 43 73 60 A I 24.20 24.40 24.60 24.80 25.00 5000 m/z 55.10 78.45% 29

m/z-> 0^^ 20 40 Abundance i ii w wuUu, ”•143157171 185i99^P227 241 T 60 80 100 120 140 160 180 200 220 240 260 #195442: Hexadecanoic acid (CAS) $S Palmitic acid $$ Palmi... ■ 43 60 ? IKhm. k.. ’’I ' ' ' ' I ’ ' ' ' I ' ’ 24.20 24.40 24.60 24.80 25.00 m/z 43.10 63.52%

m/z-> 5000

O’r 20 40 60 80 IX 97 ^29

100 120 140 160 180 200 220 240 260 L 24.20 24.40 24.60 24.80 25.00

5853.D 5080402.M Wed Apr 10 08:00:29 2002 Page 3

NYC-WTC_000060656

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NYC-WTC_000060656Source: NYC Law Department, mirrored locally

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