Water quality monitoring data sheet, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051302\11311.D Vial: 13 Acq On : 13 May 2002 9:36 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11311 5/10/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\050802.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 16 Hexadecanoic acid (CAS) $$ ... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

24.72 0.11 ug/L 116233 Phenanthrene d-10 22.53 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecanoic acid (CAS) $$ Palmi... 256 C16H3202 000057-10-3 64 2 Hexadecanoic acid (CAS) $$ Palmi... 256 C16H3202 000057-10-3 53 3 Tridecanoic acid (CAS) $$ Tridec... 214 C13H2602 000638-53-9 47 4 Glycine, N-methyl-N-(1-oxododecy... 271 C15H29NO3 000097-78-9 43 Abundance Scan 1504 (24.718 min): 11311.D (-) m/z 60.10 100.00% 60

129 5000 85

45 99 115 157171 213 256 T 1 < < ■ • 1 • ■ • ■ 1

m/z-> 0! ■. ।.... । . rr|., AL4L II ' I' " ' I ‘ 20 40 60 80 100 120 140 160 180 200 220 240 260 143 ■ I ‘" I'1'' I " 190

1’3 24.40 24.60 24.80 25.00 m/z 73.10 80.34%

Abundance #195443: Hexadecanoic acid (CAS) $$ Palmitic acid $$ Palmi... 73

5000 55

97 , 115 129

213 ■ < I ■ ‘ ■ i ■ a. 24.40 24.60 24.80 25.00 m/z 57.05 58.54% 157171185

fl yy — 256 143 I I I1?9 T 227241 L 01 ।■i>•i■1■ ■7. > > । > । > i । > < > > । । > i > , i i ■ r j ■ ■ 111 r i 11 111 “ 11'''I *" r |»> n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195439: Hexadecanoic acid (CAS) $$ Palmitic acid $$ Palmi... 43 60 AdM 24.40 24.60 24.80 25.00 5000 m/z 129.10 54.14%

831 971 115 129 m/z-> O+ 20 40 60 4 80 100 120 140143157171185199213 ’111111121112111/11111232993109223113 160 180 200 220 240 260 256 S’T Abundance #136155: Tridecanoic acid (CAS) $$ Tridecylic acid $$ n-Tr... 60 T T T ■ i ■ M ' i 24.40 24.60 24.80 25.00 m/z 55.10 53.30% 43

5000 129 29 85 171

0 14,44 Al r 44* 115 143157 199 185 214

■ > i ■ ■ •11" ■ ■ i " ■ ■ i1 • mas/mo miz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 24'46 24.60 24.80 25.00 1711

.1311.D 050802.M Tue May 14 11:10:48 2002 Page 18

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