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GCMS sample AE07110 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07110 including detection of unknown compounds.

NYC-WTC_000049027–000049062

Folder label: “GCMS X 4/12/02 A 4/23/02

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Scanned page image, NYC-WTC_000049046
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohik Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 1-Heptadecanol $$ n-Heptade... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 23.59 19.77 ug/L 2549600 Phenanthrene-d10 22.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual l 1-Heptadecanol $$ n-Heptadecanol ... 256 C17H36O 001454-85-9 94 2 1-Hexadecanol 242 C16H34O 036653-82-4 94 3 Cyclododecane 168 C12H24 000294-62-2 94 4 Cyclotetradecane 196 C14H28 000295-17-0 93 Abundance Scan 3490 (23.585 min): 7110.D (-) m/z 55.10 100.00% 55 83 69 97 5000 4'

111 1****’*’* T T | 125 23.20 23.40 m/z 23.60 23.80 57.10 24.00 90.03% 04 ——4 Tp- ’) . . t . । n r 140153 Tr ’ . 1 "T ■ । n । 168 182’196 FPIspt .......... fi-Stdttts’|t m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #195644:1-Heptadecanol $$ n-Heptadecanol $$ Heptadecyl al... 55 4 69 83 97 5000 T T T T T 111 23.20 23.40 23.60 23.80 24.00 m/z 83.10 79.59% 2‘ 125

/z-> 01 ■ • i ■ 20 440 '■ 60Mn. .4.4, 1 13% 154168182 , ■, 210 238 80 100 120 140 160 180 200 220 240 Abundance #177026:1-Hexadecanol 43 57 83 23.20 23.40 23'60 23'80 24.00 70 97 m/z 69.10 71.88% 5000 29 111 | 125 - I . ’ il . 1A1. । 139 154168182 196 224 0’ rTJ tL q .. r.! 11 i । |i 1f |i 111111111 > m/z-> 20 40 60 801 100 120 140 160 180 200 220 240 Abundance #71567: Cyclododecane 41 55 T T T T 1’1 23.20 23.40 23.60 23.80 24.00 69 m/z 43.20 65.20% 83 5000 97

n/z—> 14 1 27 0 1 »"■ 1 ‘T- 20 40 Lil 60 80 111 125 140 168 ■ i •1 ■ ■ i “ •' i “ ■ ■ i ■ ■ • • l • 100 120 140 160 180 200 220 240 23.20 23.40 23.60 23.80 24.00

7110.D 5080402BBC.M Tue Apr 23 15:52:12 2002 Page 7

NYC-WTC_000049046

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NYC-WTC_000049046Source: NYC Law Department, mirrored locally

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