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GCMS analysis results for sample AE00838, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00838 including surrogate recovery and unknown compounds.

NYC-WTC_000052187–000052204

Folder label: “GCMS X 1/11/02 A 1/31/02

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Scanned page image, NYC-WTC_000052197
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00831.D Vial: 4 Acq On : 31 Jan 2002 1:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L *********** ** ***************************************** ******* * ******* Peak Number 7 Heptadecane $$ n-Heptadecan... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

21.33 0.35 ug/L 251890 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane $$ n-Heptadecane $$ ... 240 C17H36 000629-78-7 97 2 Heptadecane 240 C17H36 000629-78-7 96 3 Heptadecane (CAS) $$ n-Heptadeca.. . 240 C17H36 000629-78-7 95 4 Heptadecane 240 C17H36 000629-78-7 93 Abundance Scan 1573 (21.333 min): 00831 .D (-) m/z 57.10 100.00% 57 71 43 85 5000

m/z—> 0— r 40 60 80 +— 100 120 99 .. . | 113 127 140 155 140 160 180 200 220 240 240 21.00 2120 21.40 21 .'60 ' m/z71.10 70.63% Abundance #174546: Heptadecane $$ n-Heptadecane $$ Normal-heptadecane 57 71 85 5000 1dIu । । ' i 1 ■ ' 1 i 1 ' ■ ’T 1 1 ' । 21.00 21.20 21.40 21.60 99 m/ z 43.10 64.14%

m/z-> ........ I 0- 1 1-,—r-r-T -r 1ru 40 60 l + 80 II ' 1 i 1 100 113 127 141 —L Tr 120 140 196 TTTnnm/m—m——TTTTT 160 180 200 220 240 240 Abundance #174551: Heptadecane 57

71 21.00 21'20 2'1'40' 21.60 1 ' 5000 m/ z 85. 10 49.26% 85

QQ

miz-> 01 PP —CndCnnImd/dmm 40 60 80 100 1

120 dl |

140 113 127 141 155 169 ,|

160 ,i

180 200 220 210 240 — 240 Abundance #174553: Heptadecane (CAS) $$ n-Heptadecane $$ Normal-hept... IMOTi , , NIvi 43 57 21.00 21.20 21.40 21.60 m/z41.10 22.80% 71

5000 85

— —— 99 113 127 141 240 WAN/P 0 ------- * /z-> 40 60 80 100 120 140 160 180 200 220 240 21.00 21.20 21.40 21.60

00831.D SCAN508.M Fri Feb 01 09:18:43 2002 Page 9

NYC-WTC_000052197

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NYC-WTC_000052197Source: NYC Law Department, mirrored locally

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