Laboratory report showing GCMS analysis of sample AE00838 including surrogate recovery and unknown compounds.
NYC-WTC_000052187–000052204Folder label: “GCMS X 1/11/02 A 1/31/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\5973N\02JAN31\00831.D Vial: 4 Acq On : 31 Jan 2002 1:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ******************************************************* ** * * **** ****** Peak Number 8 fluorene-9-spiro-cyclopropane Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.41 ug/L 297073 Phenanthrene-dl0 22.65
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 fluorene-9-spiro-cyclopropane 192 C15H12 000000-00-0 59 2 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H1203 000607-91-0 58 3 1,4-Dimethyl-3,5-propanobicyclo[... 192 C13H20O 000000-00-0 49 4 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 45 Abundance Scan 1656 (22.280 min): 00831 D (-) m/z 192.10 100.00% 192
5000
82 96 _ 146 160 22.00 22.20 22.40 22.60 42 56 70 11 122 136 | | 0 TT+TTT+THTHTtrr " i " '111" 11"1 ryurev ' r" 11111111111111 TTT m/z 191.10 16.23% n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103959: fluorene-9-spiro-cyclopropane 192
165 5000 .. Jl.. A 22.00 22.20 22.40 22.60 m/z 193.10 13.20% 87 96 0 111■■■’i1'111'111111 ........ 139 152 . ..... i111' ।1111111 "I m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102621:1 3-Benzodioxole, 4-methoxy-6-(2-propenyl)- $$ Be... 192 TITTTT 1 'I ' ' 1 1 22.00 22.20 22.40 22.60 5000 m/z 96.05 12.88% 165 89 103 119 I 134 131 147
/z-> 0 — TTnuuOuTTTr | 177 —l Abundance 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #103601:1,4-Dimethyl-3,5-propanobicyclo[2.2.2]octan-2-one 107 192 A AWw.W w , AMWA 22.00 22.20 22.40 22.60 159 m/z 146.10 11.15% 119 93 5000 132 145 174
m/z-> 0 " r " ' i' " ' I" “ 11 " 1111 " I " " I " " i1111111" I 1' i''1' i' ■ 40 50 60 70 80 90 100 110 120 130 140 150 160 1 70 180 190 200 U ‘TT u r । । 1 re / , । 2 ri 4 ■) । f 22.00 22.20 22.40 22.60
10831.D SCAN508.M Fri Feb 01 09:18:44 2002 Page 10
NYC-WTC_000052198
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NYC-WTC_000052147
Laboratory report showing GCMS analysis of sample AE00832 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052205
Instrument output file from GCMS analysis using method SCAN508 showing response for deuterated internal standards.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052088
Laboratory report showing GCMS analysis of sample AE00839 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052047
Laboratory report showing GCMS analysis of sample AE00830 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051263
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00466 conducted on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052108
Laboratory report showing GCMS analysis of sample AE00840 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052167
Laboratory report showing GCMS analysis of sample AE00838 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052128
Laboratory report showing GCMS analysis of sample AE00843 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050577
Laboratory report listing unknown compounds and surrogate recovery for sample AE00249 analyzed on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009946
Analytical results for sample AE01507 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003981
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010126
GCMS laboratory results for sample AE01638 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000052017
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
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NYC-WTC_000052018
Fragmented record showing sample volume, drip rates, and surrogate addition fields for environmental testing.
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NYC-WTC_000052020
Laboratory report detailing GCMS analysis of sample AE00830 for nitrosamines and dichlorobenzenes.
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Laboratory report showing GCMS reference analysis of sample AE00330 for nitrosamines and chlorinated compounds.
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NYC-WTC_000052029
Laboratory report showing GCMS blank analysis of sample AE00830 with compounds below detection limits.
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