Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.
NYC-WTC_000004770–000004933Folder label: “GCMS X 2/1/02 A 2/5/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB05\28324A.D Vial: 3 Acq On : 5 Feb 2002 12:22 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.18 ug/L 199897 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 64 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 59 3 9H-Fluorene, 9-ethylidene- (CAS) 192 C15H12 007151-64-6 53 4 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H1203 000607-91-0 45 Abundance Scan 1656 (22,280 min): 28324A.D (-) m/z 192.10 100.00% 1512
..... ... A 5000
96 • 146 160 । 82 22.00 22.20 22.40 22.60 m/z—> 0 42 52 TLWTTTTTH 70 106 118 132 — )mtha -H | 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 - m/z 191.10 16.24% Abundance #102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192
5000 108 -4 22.00 22.20 22.40 22.60 146 175 m/z96.00 15.82% 0 1’11111111111*0011012221- i " " I' “' i" " r ' ■ i'" ' i' "' i ■ Baunur Tmu m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192
22.00 22.20 22.40 22.60 5000 82 m/z 146.10 15.00% 54 110 30 1 94 160 0 mm mP mHmmmeet 1 '' ■11 ‘ ' i1'111 •'1111 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103905:9H-Fluorene, 9-ethylidene- (CAS) A 1912 22.00 22.20 22.40 22.60 m/z 193.10 13.30%
5000 165 99 — 83 0 .... 45........... | TTHTTTTTTTTTTTTTTTPTT 1 * I' ‘' I' " 11' ‘1' I ‘'1111111111' trmmn ........................ ................. / n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60
28324A.D SCAN508.M Fri Feb 22 11:44:13 2002 Page 12
NYC-WTC_000004873
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NYC-WTC_000003981
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004935
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010027
GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010927
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036779
GCMS analysis report for sample AD29522 listing unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052108
Laboratory report showing GCMS analysis of sample AE00840 including surrogate recovery and unknown compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050664
Laboratory report listing unknown compounds and surrogate recovery for sample AE00165 analyzed on February 13, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009966
Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010106
GCMS laboratory results for sample AE01637 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052069
Laboratory report showing GCMS analysis of sample AE00833 including surrogate recovery and unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000004769
Fragmented GCMS document excerpt from February 2002, related to World Trade Center environmental activities.
Filed in the same folder
NYC-WTC_000003981
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
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NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
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NYC-WTC_000004935
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
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NYC-WTC_000010027
GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
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