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GCMS DFTPP calibration report, Feb 5 2002

Machine-extracted title · confidence 95%

Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

Page image
Scanned page image, NYC-WTC_000004873
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB05\28324A.D Vial: 3 Acq On : 5 Feb 2002 12:22 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.18 ug/L 199897 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 64 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 59 3 9H-Fluorene, 9-ethylidene- (CAS) 192 C15H12 007151-64-6 53 4 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H1203 000607-91-0 45 Abundance Scan 1656 (22,280 min): 28324A.D (-) m/z 192.10 100.00% 1512

..... ... A 5000

96 • 146 160 । 82 22.00 22.20 22.40 22.60 m/z—> 0 42 52 TLWTTTTTH 70 106 118 132 — )mtha -H | 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 - m/z 191.10 16.24% Abundance #102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

5000 108 -4 22.00 22.20 22.40 22.60 146 175 m/z96.00 15.82% 0 1’11111111111*0011012221- i " " I' “' i" " r ' ■ i'" ' i' "' i ■ Baunur Tmu m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192

22.00 22.20 22.40 22.60 5000 82 m/z 146.10 15.00% 54 110 30 1 94 160 0 mm mP mHmmmeet 1 '' ■11 ‘ ' i1'111 •'1111 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103905:9H-Fluorene, 9-ethylidene- (CAS) A 1912 22.00 22.20 22.40 22.60 m/z 193.10 13.30%

5000 165 99 — 83 0 .... 45........... | TTHTTTTTTTTTTTTTTTPTT 1 * I' ‘' I' " 11' ‘1' I ‘'1111111111' trmmn ........................ ................. / n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

28324A.D SCAN508.M Fri Feb 22 11:44:13 2002 Page 12

NYC-WTC_000004873

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NYC-WTC_000004873Source: NYC Law Department, mirrored locally

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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