GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB05\28324A.D Vial: 3 Acq On : 5 Feb 2002 12:22 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 Methenamine $$ 1,3,5,7-Tetr... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 16.55 0.04 ug/L 45408 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Methenamine $$ 1,3,5,7-Tetraazaa... 140 C6H12N4 000100-97-0 25 2 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 17 3 1,3,5,7-Tetraazatricyclo[3.3.1.1... 140 C6H12N4 000100-97-0 9 4 3H-Pyrazol-3-one, 2,4-dihydro-2,... 140 C7H12N20 003201-25-0 9 Abundance Scan 1154 (16.549 min): 28324A.D (-) m/z 140.20 100.00% 140

5000 122 172 _■ i ■___ _ 1 ■ । ' 1 ■ ■ i 1 ' ■ ■ • i ■ । 43 56 71 89 16.20 16.40 16.60 16.80 - m/z-> 0- 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 4l... -.... | T‘[1 m/Z 172.20 28.48% Abundance #35198: Methenamine $$ 1,3,5,7-Tetraazaadamantane$$ 1,3,5." 42

5000 140 16.20 16.40 16.60 16.80 '' m/z 122.10 27.36% 15 71 85 112

Z-> 0 i 39H TTUTTDUOTTTTTETTTTTTT 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 " ।" i ‘। ■11 ■ i'

Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 140

16.20 16.40 16.60 16.80 5000 m/z 138.20 22.75% 44 71 123 86 96 112 0- - 11 " 11 rmh) " i " " i " " i “ " i' nz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35204:1,3,5,7-Tetraazatricyclo[3.3.1.1 (3,7)]decane (CAS)... 42 16.20 16.40 16.60 16.80 m/z 136.10 19.18% 5000

140

O-r i TTIM i । ' i n । '''11"1'61i'" 11’7.1’1 । r <-| 1111 85 j 111111. > >112 11,.. ।, j 11 " i " " i11" r " 11' 1 ■ । ■ 1 1 ■ i ■ ■ n”1 ' 1 1 I ' 1 1 ' i ' m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 16.20 16.40 16.60 16.80

28324A.D SCAN508.M Fri Feb 22 11:44:13 2002 Page 11

NYC-WTC_000004872

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