DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004494–000004704

Folder label: “GCMS X 1/30/02 A 2/26/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB26\02088.D Vial: 5 Acq On : 26 Feb 2002 6:06 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 2,4(1H,3H)-Pyrimidinedione,... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 16.55 0.04 ug/L 27754 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,4(1H,3H)-Pyrimidinedione, 1,3-... 140 C6H8N202 000874-14-6 7 2 Methenamine 140 C6H12N4 000100-97-0 7 3 URACIL DIMETHYL 140 C6H8N2O2 000000-00-0 7 4 1,3,5,7-Tetraazatricyclo[3.3.1.l... 140 C6H12N4 000100-97-0 7 Abundance Scan 1167 (16.548 min): 02088. D (-) m/z 140.10 100.00% 140 4 5000

43 56 122 172 71 89

m/z-> Abundance 0 m ■ i " " i' 1 "r' 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 " i " " i11" i " " i1

#35146:2,4(1 H,3H)-Pyrimidinedione, 1,3-dimethyl- $$ Uraci... 16.20 16.40 16.60 16.80 m/z 138.10 25.64%

140

55 5000 83 1 ' i ' 1 1 ' i ■ ' ' ' i ' ' ' ' i ' 16.20 16.40 16.60 16.80 m/z 172.20 23.45%

m/z-> 0 TTPTTT m 96 111 ir......1" ■ i " " i ■ ■ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 1' i ■'।11 ■ ■ ।11' ■ i ’

Abundance #35197: Methenamine 42 .................... II...................... 16.20 16.40 16.60 16.80 5000 m/z 136.00 19.00% 140

15 27 h 71 85 112 0- " I I " " I " " i' Wj-r TTWTTWTTTTTTPTTITTTIT ‘11′211111711111/11 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35156: URACIL DIMETHYL ..................................................... .. 140 16.20 16.40 16.60 16.80 m/z 43.00 18.96% 55 5000 83 N

42 96 111 0 —mm I+.. rp *' I " " 111'' I 1 “ I' ‘ miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 16.20 16.40 16.60 16.80

02088.D HP022102.M Wed Feb 27 08:35:15 2002 Page 13

NYC-WTC_000004641

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NYC-WTC_000004641Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999