GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\00003A.D Vial: 2 Acq On 5 Feb 2002 3:46 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 10 Pyrimidinetetramine- $$ Pyr... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T.

16.55 0.05 ug/L 59892 Acenaphthene-dl0 18.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 23 2 meta-Methoxybenzenethiol $$ 3-Me... 140 C7H80S 015570-12-4 9 3 Cyclohexanone, dimethylhydrazone. .. 140 C8H16N2 010424-93-8 9 4 .beta.,beta.-Difluorostyrene 140 C8H6F2 000000-00-0 9 Abundance Scan 1154 (16.549 min): 00003A.D (-) m/z 140.20 100.00% 140

5000

43 56 71 122 172 89 r ' i ■ ' ■ ' i ' ' ' i 1 ' ' 1 i ' 1 ' ' i ' 16.20 16.40 16.60 16.80

n/z-> 0- m— 1 i L 40 50 60 70 80 90 100 110 120 130 140 150 160 170 I 1 ' ‘ ‘ ' 1 1 ‘ J 1)1 m/z 138.10 26.04% Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 140

5000 IT 16.20 16.40 16.60 16.80 44 71 123 m/z 122.10 24.85%

0- ...40H...50....... IImm 86 96 112 I 1 1 ' f I I • I I I I I I * I m/z-> 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35298: meta-Methoxybenzenethiol $$ 3-Methoxythiophenol $$... 140 ■ ' i ' 1 ' ' i ' r 1 1 1 1 1 1 1 1 1 16.20 16.40 16.60 16.80 5000 rn/z 172.20 24.06% 97 125

66 , , 110

miz-> 0- ‘ ■ i' ■ 1 ■ i1 40 50 .... 1..... 84,1. 60 70 80 — TH I 1 ‘’1 I ' 1 11 ! 90 100 110 120 130 140 150 160 170 P .... ................. ).............................. Abundance #35946: Cyclohexanone, dimethylhydrazone (CAS) $$ Cyclohex... 44 140 16.20 16.40 16.60 16.80 m/z 71.10 23.31%

5000 96 125 67 84 0 TIII -P— 60 70 -H I........... I P J___________ __ ■ i ■ ■ ■ ■ i > 1 1'' 11 1 ■ ■ I' '1 ‘1′11111 "tI Ur m/z-> 40 50 80 90 100 110 120 130 140 150 160 170 16.20 16.40 16.60 16.80

00003A.D SCAN508.M Thu Feb 21 10:18:51 2002 Page 12

NYC-WTC_000004815

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