DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004494–000004704

Folder label: “GCMS X 1/30/02 A 2/26/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02FEB26\02091.D Vial: 8 Acq On : 26 Feb 2002 8:34 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 10 2,4(1H,3H)-Pyrimidinedione,... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 16.55 0.03 ug/L 30191 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,4(1H,3H)-Pyrimidinedione, 3,6-... 140 C6H8N202 019674-60-3 7 2 2,4(1H,3H)-Pyrimidinedione, 1,3-... 140 C6H8N202 000874-14-6 7 3 Pyrazine, 2-methyl-3-(methylthio... 140 C6H8N2S 002882-20-4 5 4 Methylphloroglucinol 140 C7H803 000000-00-0 5 Abundance Scan 1167 (16.548 min): 02091 .D (-) m/z 140.10 100.00% 140

5000 122 172 ii 44 56 71 84 16.20 16.40 16.60 16.80 . .......... ... I..,..I..... . ... ■ ■ i ■' ■' i ‘ ‘ i ■ ■ ■ ■ i TT-p-T ' ' I ' 1 ' ' I 1 1 ' ' I TT-p m/z 122.10 36.33% mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35148:2,4(1 H,3H)-Pyrimidinedione, 3,6-dimethyl-$$ Uraci... 42 140 5000 68 83 16.20 16.40 16.60 16.80 m/ z 172.10 35.65% 27 54 , 110 oV ‘I - ----- !............................ 1'1' i'1111111 ■ i' ■ ■ ■ i1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35145: 2,4(1 H,3H)-Pyrimidinedione, 1,3-dimethyl- 42 140 ....... ............ .......... 55 16.20 16.40 16.60 16.80 83 5000 m/z 138.00 25.17%

27 — i - ‘II TTTITLTIPTTTITTTTTTT96 111 0- TT m/z- > 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35175: Pyrazine, 2-methyl-3-(methylthio)- (CAS) $$ 2-Meth... .................... II...................... 140 16.20 16.40 16.60 16.80 m/ z 71.00 17.13%

5000 107 N 42 125 84 94

/z-> 0j . . . . । . . . . । TTTTTT _ 20 30 40 50 60 70 80 66 ..... ■ i ■1'' ।1 ■ ■ i1 ,

+ 90 100 110 120 130 140 150 160 170 1' 111'11'11' i " '111 ... 11... 16.20 16.40 16.60 16.80

02091.D HP022102.M Wed Feb 27 08:35:34 2002 Page 12

NYC-WTC_000004700

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999