DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004494–000004704

Folder label: “GCMS X 1/30/02 A 2/26/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB26\02091.D Vial: 8 Acq On : 26 Feb 2002 8:34 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 26, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ******************************************************************** * Peak Number 11 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 115040 Phenanthrene-dl0 22.64 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY- .BETA. -METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 3 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 4 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 45 Abundance Scan 1675 (22.283 min): 02091 .D (-) m/z 192.00 100.00% 192

5000 -.......... — 96 82 146 160 22.00 22.20 22.40 22.60

m/z—> 0 —PPTHm 42 70 -- H aljenirul 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 120 m/z 191.00 18.87% Abundance #102588: 4-METHOXY-.BETA.-IVIETHYLCINNAIVIIC ACID $$ 2-Butenoi... 192

5000 108 .... n... a 22.00 22.20 22.40 22.60 146 175 m/z96.00 17.98%

m/z-> 0 111' “ ' i " “ I " '111''11" 111 H " I " " I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 i1 " 11" " r " ' i1' ' i " " i “ " i' .. TTI 4 Abundance #88409: N-perdeuteriobenzylideneaniline 192 ■ ■ i ■ 1 ' ■ i ■ 22.00 22.20 22.40 22.60 5000 82 m/z 146.10 16.17% 54 110

/z—> 30 0 ""I...... . " I " " I' 1 94 160 mH TTTTTTTTTTTTTETTTTTTTTTTTTTTTTTTTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 4 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene ................... ■ ■ i ■ ■ 192 22.00 22.20 22.40 22.60 m/z 193.00 13.95% 5000

96 165 88 J 139 152 | 176 0 I ' “ ' I " ' ' I " " I " " I " ‘ ' I " ' 1 I 1 1 । 1 I ' " 1 I " " I 1 ' " I " "‘I 1 " 1 I 1 " 1 I ‘'t ■ I | I I I ! | 1 I l'l I1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

02091.D HP022102.M Wed Feb 27 08:35:34 2002 Page 13

NYC-WTC_000004701

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999