GCMS analysis log for sample AE00699 showing surrogate recovery and unknown compounds detected on January 29, 2002.
NYC-WTC_000052001–000052016Folder label: “GCMS X 1/10/02 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\O2JAN16\00699.D Vial: 4 Acq On : 16 Jan 2002 1:20 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************* * * * ****** * * * Peak Number 8 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
22.28 0.14 ug/L 74636 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H12O3 019169-94-9 72 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 59 3 1,2-Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 53 4 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 Abundance Scan 1656 (22.280 min): 00699. D (-) m/z 192.10 100.00% 192
5000
* 22.00 22.20 22.40 22.60 0 !! | I ™ 82 ? ”6 160 I | I I I . | I ! . > .1 I rprer | < I I | I I I I | I I I < m+rpi . ( . I | ! ! I I | I ! I I | I i'l . | I I I . m/z 191.10 16.87% /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192
108 5000 ‘18 i ■ ■ 1 22.00 22.20 22.40 22.60 146 175 m/z 193.10 16.27%
0 '' i ■' ■' i1' ■' i'''11' ■'' r ■ " I'''' I i " " 11'1' 1 I''' ’ I tumn m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192
22.00 22.20 22.40 22.60 5000 82 m/z 146.10 13.80%
54
m/z—> Abundance 30 0 TTTTPTT " i " " i " " i -HP 94 110
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 160 . ................ ■' ■ i....................."‘I #102107:1,2-Phenylene diisothiocyanate u "TI 192 22.00 22.20 22.40 22.60 m/z 96.10 13.33% 64 5000
75 90 134
m/z-> 0 " ।' i" " i ,1.7....,14197 TTT 107
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 'i"" r1 "i 160 4— TTT 22.00 22.20 22.40 22.60 T
00699.D SCAN508.M Thu Jan 17 08:17:01 2002 Page 10
NYC-WTC_000052014
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NYC-WTC_000051984
GCMS analysis log for sample AE00740 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051567
Laboratory report showing GCMS analysis results for sample AE00562 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052128
Laboratory report showing GCMS analysis of sample AE00843 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050558
Laboratory report listing unknown compounds and surrogate recovery for sample AE00248 analyzed on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051364
Laboratory report showing GCMS analysis of sample AE00314 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051024
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 8-10, 2002 testing.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051642
Laboratory report showing GCMS analysis results for sample AE00616 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050205
Laboratory report documenting GCMS analysis of sample AD31647 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051040
Laboratory report showing GCMS analysis of sample AE00276 for unknown compounds and DDD on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050500
Laboratory report for sample AE00168 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052108
Laboratory report showing GCMS analysis of sample AE00840 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010027
GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000051782
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000051783
Technical log recording method parameters and sample processing details for a DEP laboratory procedure between January 10 and 16, 2002.
Filed in the same folder
NYC-WTC_000051785
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051789
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051794
GCMS analysis log for sample AE00703 showing blank results with compounds below detection limits on January 16, 2002.
Filed in the same folder