GCMS results for sample AE00699, Jan 29 2002

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GCMS analysis log for sample AE00699 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000052001–000052016

Folder label: “GCMS X 1/10/02 A 1/16/02”

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Data File : C: \MSDCHEM\1\5973N\02JAN16\00699.D Vial: 4 Acq On : 16 Jan 2002 1:20 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 2-Propanol, 1-butoxy- (CAS)... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 8.24 0.20 ug/L 65014 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-butoxy- (CAS) $$ 1... 132 C7H16O2 005131-66-8 56 2 Morpholine (CAS) $$ BASF 238 $$ ... 87 C4H9NO 000110-91-8 35 3 Morpholine (CAS) $$ BASF 238 $$ ... 87 C4H9NO 000110-91-8 25 4 Morpholine $$ p-Isoxazine, tetra... 87 C4H9NO 000110-91-8 25 Abundance Scan 426 (8.237 min): 00699.D (-) m/z 45.10 100.00% 45 57

5000 87 41

7.80 8.00 8.20 8.40 8.60

n/z-> 0b 5 4 | I " ,TT 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 A i ■ * ■ ■ i ■1 ■ • i ■ ■ ■ ■ r m/z 57.10 90.64% Abundance #28054:2-Propanol, 1-butoxy- (CAS) $$ 1-N-BUTOXY-2-PROPAN... 45 57

5000 11i1111r11’ 1 r1 ■ ' ■ । ■ 1 7.80 8.00 8.20 8.40 8.60 27 31 87 m/ z 87.10 47.19% 61 75 Of ■' i " " i11" 111111 ■ .... . 1 11" 11" " I " 111" " I "‘I i1111111 THHHrrrm m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4372: Morpholine (CAS) $$ BASF 238 $$ Diethylene oximide ... 29 57 7.80 8.00 8.20 8.40 8.60 5000 m/z 41.10 35.52% 87 15 42 26 ob ′′′′′′′′′′′′ i " " i'' " r " ' i 11. ...... . ।।।। —uxrltli m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4375: Morpholine (CAS) $$ BASF 238 $$ Diethylene oximide ... 57 N...... 7.80 8.00 8.20 ' I”’ 8,40 "I 1 1 1 8.60 29 m/z 56.10 32.35% 87 5000

m/z-> °b 5 " i ‘■ i" ■ ■ i1 A Hyrr 11 । । i r} 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ।1| | । | | 1 I 1 I |’I " ! | HTpo 7.80 8.00 8.20 1 । r1 1 11 r1 1 8.40 8.60

)0699 .D SCAN508.M Thu Jan 17 08:17:01 2002 Page 9

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