DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB01\30704.D Vial: 1 Acq On 1 Feb 2002 2:44 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 2-Propanol, 1,1'-oxybis- (C... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 9.56 0.13 ug/L 47418 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1,1'-oxybis- (CAS) $... 134 C6H14O3 000110-98-5 50 2 2-Propanol, 1,1'-oxybis- (CAS) $... 134 C6H14O3 000110-98-5 39 3 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 9 4 BIS(1-METHYL-2 -HYDROXYETHYL)ETHER 134 C6H14O3 000000-00-0 9 Abundance Scan 542 (9.562 min): 30704. D (-) m/z 59.10 100.00% 59

5000

011... 45

I 51 73 103

III l 1.......................................................................... ■ ’ i ' ■ ■ ' i ' ' 1 ■ i 1 ■ ■ ■ i ■ 1 ‘ ■ i 1 ■ ■ 1 i ' ' 1 ■ i 1 ■ ' ' i ' ■ 1 ‘ i 1 ■ ■ ' i ' 1 ' 1 i ■ 9.20 m/ z 9.40 45.10 _M. 9.60 9.80 42.50% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #29204:2-Propanol, 1,1‘-oxybis- (CAS) $$ Dipropylene glyc... 59

31 5000 45 103 9 20 9.40 9.60 9.80 m/z 103.10 32.63%

miz-> .. 1 , 0 1 1 1 1 ' 1 1 1 1

Abundance 20 30 40 n napnil1 i ■ ' ' ■ i ■ ■ ' ■ i ' 1 1 1 i ‘ ' 1 ■ i ■ 1 ■ ■ i ' ' 1 ■ i ■ ■ ' ■ i ■ ' 1 1 i ■ 50 (60 70 80 90 100 110 120 130 140 #29205: 2-PropanoI, 1,1 ’-oxybis- (CAS) $$ bipropylene glyc... 59 31 920 9.40 9.60 9.80 5000 45 m/z 73.10 30.12% 103

..Il .. II ... .......... 0 ■ I ' ' ■ • i ■ 1 ‘ ■ i 1 11 ' i ‘ ■ ■ ■ i ■ ■ ■ ■ i ' ' ■ ■ i 1 ■ ■ ■ i ' ‘ 1 1 i ■ i • ■ i ■ ■ ■ ■ i ' ■ ■ ■ । ■ ■ ■ ■ । ■ miz-> Abundance 20 30 40 50

59 60 70 80 #61826:2-Butanol, 3,3’-oxybis- 90 100 110 120 130 140

9.20 9.40 NNM. ‘ ' I ‘ 9.60 ■ I 1 ‘ 9.80 ' I '

m/ z 41.10 22.06% 5000 31 45 103

134 O—PTTT 1 74+ T I 1 I'1 ■ ■ ■ i ' ■ ■ ■ i 1 ■ ■ ' i ■ ■ ■ ■ i ' 1 ■ । I 1 1 ' 1 I 1 1 ■ ' I ' 1 ' m/z—> 20 30 40 50 (60 70 80 90 100 110 120 130 140 9.20 9.40 9.60 9.80

30704.D SCAN508.M Mon Feb 04 08:41:25 2002 Page 5

NYC-WTC_000004117