DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000003981–000004147

Folder label: “GCMS X 1/29/02 A 2/1/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB01\30704.D Vial: 1 Acq On : 1 Feb 2002 2:44 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 2 1,3-Dioxolane, 2-heptyl- Concentration Rank 3 . R.T. EstConc Area Relative to ISTD R.T. 5.93 0.47 ug/L 175224 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxolane, 2-heptyl- 172 C10H20O2 004359-57-3 37 2 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 3 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 4 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 Abundance Scan 224 (5.931 min): 30704.D (-) m/z 73.10 100.00% 73

5000

43 5.60 5.80 6.00 6.20 111.155.... 1 .......87....... 103................ . ................................ O-PTT ■ ’ ■ ।11 ■11' ■ ■ ■ ।1' 1 ■ । ■ m/z 43.10 22.19%

.. 1 . nlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #76647:1,3-Dioxolane, 2-heptyi- 73

5000 5.60 5.80 6.00 6.20 m/z 45.10 11.68% ..... — 45 ........................................

m/z-> 0- • । •11 'I ■1 ■ ■ i1 ■ ■ ■ । ■ ’14 ।1 ■ ■ ■ ।' 20 30 40 50 60 70 +41 99 TIPuuuuDTT ' i " 1 ■ i'' ‘' i 171 80 90 100 110 120 130 140 150 160 170 180 Abundance #9663: 3-Pentanol, 3-methyl- 73 5.60 5.80 6.00 6.20 5000 m/z 41.10 8.94%

55 45 87 27 0- ‘i'■ ■' i‘1 ‘ 114 "11' Tp h ‘ I ' 1’i 10* li 11 miz- > 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 5.60 5.80 6.00 6.20 m/z 71.10 8.26%

5000 43 27 87 0 pr 'T'55 , i 113 174 1 “ I' । ■ 'T' TTTT TTTTTT—TTgTTTTTTTI ‘1 " I' ' ■ i ■ ' • ■ i ■ ■ ' 1 i ' ‘ ' 1 i ■ ' ■ ' i m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

30704.D SCAN508.M Mon Feb 04 08:41:24 2002 Page 4

NYC-WTC_000004116

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999