DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB26\0130B.D Vial: 1 Acq On : 26 Feb 2002 10:17 am Operator: Sample : lab blank 1/30 Inst : Instrumen Mise : February 26, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Acetic acid, 3-[1,3]dioxola... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.95 0.38 ug/L 192933 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 38 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$. . . 174 C8H14O4 015745-87-6 38 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 4 1,3-Dioxolane, 2-heptyl- 172 C10H20O2 004359-57-3 9 Abundance Scan 228 (5.948 min): 0130B.D (-) m/z 73.10 100.00% 73

5000 43 TIdd 1′1+‘ II IfTr i > i T-i 5.60 5.80 6.00 6.20 O-PTT -55 ll "i ■' i' ■ 87 103 m/ z ‘ ' I' ' I ‘ ■' i 11'11''''' i11'' i11' ■ i1' 1 1111 111'11 1 1111111'1 111 43.10 25.39% nlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 ___ Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 1 ' I ' ' ' ' I MA AAi A, I 1 ' 5.60 ' 5.80 6.00 6.20 43 m/ z 45.10 10.50% 27 55 , 87 113 174 0-- 11 " 1 ■ i'' ■' T' 1 ■' i''1 11 ' ■11 r 1 ■1111'' i1 '1 ■ i ■'1 ' ।11 111111 1 I'11' r11 111 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 ' ' i ' ' * ' i 1 ■ 1 1 । > > > > । > 5.60 5.80 6.20 5000 m/ z 41.10 9.34% 43 27 55 87 113 174 0- ■ i ■ ■ ■ ■ । ■ TT4 ■ ।11'' ।1 ■111 ■ —TT T1101110011111110-u—-mum—u1mT ‘ /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9663:3-Pentanol, 3-methyl- 1 । I 1 1 । > i 1 73 5.60 5.80 6.00 6.20 m/z 71.00 6.97% 5000 55 45 87 27 0 1 r 1 ■'I I, ’1' '1J . . .1.................... 1 “ 11 1 TT 1 ■' i ■1'' i ■11 ■ i11 ■ ■ i ■ ‘■ i1 ■11111'1111111111111 m 1111' 11 T-r-j-r-r-r-r-j-1 /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

0130B.D HP022102.M Wed Feb 27 08:34:18 2002 Page 7

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