GCMS analysis results for sample AE00101, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN23\00101.D Vial: 4 Acq On : 23 Jan 2002 5:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.92 0.33 ug/L 107455 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 45 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 45 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 4 1,3-Dioxolane, 2-heptyl- 172 C10H20O2 004359-57-3 9 Abundance Scan 223 (5,920 min): 00101.D (-) m/z 73.10 100.00% 73

50001 43 TTI 5.60 5.80 6.00 6.20

niz-> ..... I.R +p 0- • i ‘ ■1 • i •1 • ■ i11 ‘' i' ■ ‘ ‘ i ‘1 ‘' i1 H i ‘ 87 ‘ i1 • ‘ ■ i1 “ • i “ > ■ i ■ ■ " i ■ “ ■ i “ “ i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 T" m/z 43.10 22.24% Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 ......... H .......... A . . ■ ■ ■ । • • ■ ■ । ■ ■ ■ * । • ■ ■ ■ । ■ ■ ■ ■ । 5.60 5.80 6.00 6.20 43 m/z 45.10 10.76% 27 55.... ,, , 87 113 0 Tpp11’2110111111'I > . I . . 1'. ! > . . . | . . . . | 1-1 . . | . 1 . ! I M I J l , I . j , W . I M b l p l , , | . 174 niz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-yipropyl ester 73 —M 5.60 5.80 ‘ ‘ I ‘ 6.00 ' I ‘ ' 6.20 ‘ I

5000 m/z 41.10 10.04% 43 27 55 , 87 113 174 0- I 1 1 ''' I ' 1 ' 1 l'1 1 ■ i “ ■ ‘ i “ ■ ’1’I 1 ■ ‘ I ‘ '1 ' I ‘ ‘ " I' ' ' ' !1 ri 11 11 11 111 । 11 i 1111 11 । 111 i rp 11111 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9663:3-Pentanol, 3-methyl- ■ ■ ■ i ■ ■ ■ ' i ■ ■ ■ 1 i ‘ ‘ i ■ ■ ■ ■ i 73 5.60 5.80 6.00 6.20 m/z 71.00 8.97%

5000 55 45 87

n/z-> 27 l 0- ■ i •'1 I ■ i . ■ • ’ 1- l.. ।. i1. > । <. 11 j > > i > । >, ।. 111111

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 i" ■ • i • " ■ i' ■ ■ ■ i 1’ ■ • i 1 1 ■ • i ■ 1 ■ ■ i • • ■ • i ■ • ' ■ i 5.60 5.80 6.00 6.20

00101.D SCAN508.M Thu Jan 24 09:57:14 2002 Page 7

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