GCMS analysis results for sample AE00100, Jan 2002

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Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050354–000050369

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02JAN23\00100.D Vial: 3 Acq On : 23 Jan 2002 4:36 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\i...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.90 2.02 ug/L 736773 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 2 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 33 3 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 4 N-Ethyl formamide $$ N-Formylethy. . . 73 C3H7NO 000627-45-2 9 Abundance Scan 221 (5,897 min): 00100. D (-) m/ z 73.10 100.00% 73

5000 43 *1*’’I’’* 1’* * 1 > ■ 5.60 5.80 6.00 6.20

niz-> 0-—PTTPT I I 55 .1 + 87 103 . .\ ।।।।.... ।.... ।.... ।.।.... ।.. >. । 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 I’ m/z 43.10 24.01%

Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 ‘ ■ i ■ ‘ 5.60 5.80 6.00 6.20 43 m/z <45.10 9.62% 27 0- । I । । i1' 1 “ ■ 87 55.... .1 113 174 — i■■ ■11" i1 ■ ■ ■ 11 ■ ■ ■ i■' ■ ■ i■ " ■ i■■ ■ ■ i■'"i■ h . i.... i... ’14 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #17065:3-Pentanol, 2,4-dimethyl- 73 P41 ■ ■ i • ■ ‘ ' i ■ ■ ■ ■ i • ■ ‘ ■ 5.60 5.80 6.00 6.20 5000 55 m/z i41.10 8.77% 43 27 Ii... 1Im 0- i । i i i i । i i i i j I Il I III 83 .. ।....।....।....।....।.... ।.... ।.।..।... 1111.. ।....।. miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester ■ ■ i 1 ' ■ ■ i ' ' 73 5.60 5.80 6.00 6.20 m/z 71.10 6.45% 5000 43 27 . 55 i 87 113 174 0J ■ i ■ ■" i ■ TMPP I" 11 — TAT miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

00100.D SCAN508.M Thu Jan 24 09:57:10 2002 Page 6

NYC-WTC_000050363

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NYC-WTC_000050363Source: NYC Law Department, mirrored locally

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NYC-WTC_000050240

Laboratory report documenting GCMS analysis of sample AD31646 with detection of unknown compounds and surrogate recovery.

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