GCMS analysis results for sample AE02713, March 5 2002

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Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02713 including surrogate recovery.

NYC-WTC_000010867–000010886

Folder label: “GCMS X 2/5/02 A 2/28/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB28\02713.D Vial: 3 Acq On : 28 Feb 2002 12:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.94 0.35 ug/L 130387 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 50 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 50 3 N-Ethylformamide $$ N-Formylethy. . . 73 C3H7NO 000627-45-2 9 4 Pentane, 3-methoxy- $$ 1-Ethylpr... 102 C6H140 036839-67-5 9 Abundance Scan 227 (5.936 min): 02713.D (-) m/ z 73.10 100.00% 73

5000 43 ‘ 1 l ‘ ‘ ‘ i ' ' ■ ■ i ■ ■ ‘ ■ T ■ ■ • ■ i 5.60 5.80 6.00 6.20 0--pmmmmp 1 1 55 .i........ ii । 86 “ >11' 1—mmp—mmmm0mpmempp m/z 43.10 22.66% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 ■ ■ i ' ■ ■ ■ i ‘ ■ 5.60 5.80 6.00 6.20 43 m/z 41.10 11.55% 27 55 , 87 113 174 0 TI ■ i ■ “ • i ■ “ ■ , i । ‘ 1 ■ ■ i ■'1 • i ■ ■" i • “ ■ i “ i ‘ “ i' “ • I'1 “ i “'11" ‘ ‘ i'1 •' i' miz-> 10 20 30 40 50 60 70 K) 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 34[1,3]dioxoian-2-ylpropyl ester 73 ■ • i • ' ■ ■ r1 1 1 r’ 1 1 1 i 1 ' ' 1 1 5.60 5.80 6.00 6.20 5000 m/z 45.00 8.44% 43 27 55 , 87 113 174 0-Tpp TITTTTTTE’2-'i.. ।. i'. ।.... (. i. । .-i 1111 n 111 UTTFTTTi UT7 PT1 11111 miz-> 10 20 30 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... ' ■ i ■ ■ ■ ■ i • ■ ■ ‘ i ■ • ■ ■ i ' ■ ■ • i 30 5.60 5.60 6.00 6.20 73 m/z 71.00 6.85% 5000 44 58

m/z—> 0 m 15 r TTuppmmmRTTTpr 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 ■ ■ i ‘ 5.60 • i ■ 1 > • i 1 ‘ 5.80 6.00 ■ i ■ ■ ■ • i 6.20

02713.D HP022102.M Fri Mar 01 10:06:53 2002 Page 9

NYC-WTC_000010879

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GCMS analysis results, sample AE02719, March 2002 · Box DEP Box 14

NYC-WTC_000010987

Gas chromatography-mass spectrometry analysis of sample AE02719 performed March 5, 2002, reporting other unknown compounds and surrogate 2,4-DDD recovery data.

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