GCMS analysis results for sample AE02713, March 5 2002

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Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02713 including surrogate recovery.

NYC-WTC_000010867–000010886

Folder label: “GCMS X 2/5/02 A 2/28/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02FEB28\02713.D Vial: 3 Acq On : 28 Feb 2002 12:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 6 Dodecahydropyrido[1,2-b]iso... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 5.51 0.03 ug/L 11950 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Dodecahydropyrido[1,2-b)isoquino. .. 207 C13H21NO 000000-00-0 5 2 5-Methyl-2-phenylindolizine 207 C15H13N 036944-99-7 5 3 Hexahydropyridine, l-methyl-4-[4... 207 C12H17NO2 094427-47-1 5 4 Pyrido[2,3-d]pyrimidine, 4-pheny... 207 C13H9N3 028732-75-4 5 Abundance Scan 189 (5.507 min): 02713.D (-) m/z 207.00 100.00% 2(7 A

5000

86 AAAALMA ' 5.20 5.40 5.60 5.80 ‘'1 0 I . . | .... । .... । .. > . ।.... । . 11 . |.... (.... । . rri | (■ i i । i r> > ।. r i i ।! u I | uti p 1111 I 11 111 1 I 11 u !‘8 m/z 208.00 24.44% miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #125788: Dodecahydropyrido[1,2-b]isoquinolin-6-one 207 84

5000 T-r-j-TT ■ | 1 ■ ■ । | । | 97 192 5.20' 5.40 5.60 5.80 67 109 125 178 m/z 85.90 12.63% 138 152 0: .. 11.... 1.... I.... I.. . I '■l‘“ 1—40111404114 I.. “ I “ I “11! “ 1 ‘‘ I’’ miz-> 40 50 60 70 80 90 100 110120 130 140 150 160 170 180 190 200 210 Abundance #125908:5-Methyl-2-phenylindolizine 2(17 ■ ■ ■ i ■ • • • i ■ 1 ' ■ f1 1 1 1 1 1 1 1 1 I 5.20 5.40 5.60 5.80 5000 m/z 83.90 1.05%

102 130 167 178 191 , MyMWMAWIo 04verpeitipoimmmmtpnipmmnjuir i 1111 11111 rt 11111,11 ru . । n n j n i'i 11 i I'l'] i rn |lli.i||-i‘ i “ “ m/z~> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #125674: Hexahydropyridine, 1-methyl-4-[4,5-dihydroxyphenyl- - • t ■ • ■ ■ i i i 1 ‘ i ■ * ।, । 11 11 ( 2(7 5.20 5.40 5.60 5.80 70 42 97 5000 82 136 123 150 192 0- TII1 TIVWmpgm pompopmpo p-rr ’*1’14*11444 • “ I ‘' ______________ 1______ i

miz—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210

02713.D HP022102.M Fri Mar 01 10:06:53 2002 Page 8

NYC-WTC_000010878

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GCMS analysis results, sample AE02719, March 2002 · Box DEP Box 14

NYC-WTC_000010987

Gas chromatography-mass spectrometry analysis of sample AE02719 performed March 5, 2002, reporting other unknown compounds and surrogate 2,4-DDD recovery data.

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