GCMS analysis report for sample AE01547, March 2002

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GCMS laboratory results for sample AE01547 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010066–000010085

Folder label: “GCMS X 1/23/02 A 2/21/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB21\01547.D Vial: 3 Acq On : 21 Feb 2002 4:52 pm Operator: Sample : 508 scan Inst : Inst rumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 2-(1’-METHYLINDOL-3'-YL)ETH... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 5.51 0.04 ug/L 15127 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-(1'-METHYLINDOL-3'-YL)ETHENE-1... 207 C13H9N3 065037-75-4 5 2 Hexahydropyridine, l-methyl-4-[4... 207 C12H17NO2 094427-47-1 5 3 Pyrido[2,3-d]pyrimidine, 4-pheny... 207 C13H9N3 028732-75-4 5 4 Dodecahydropyrido[1,2-b]isoquino. .. 207 C13H21NO 000000-00-0 5 Abundance Scan 189 (5.507 min): 01547.D (-) m/z 207.00 100.00% 207

5000 86 96 ‘ i • ' • * i 5.20 5.40 5.60 5.80 01 mmmpp Tp-rTTjTTTTpT-TTpn-rrp-rTTpvTTTTTTTpnnTYr^^ T’T m/z 85.90 43.78% iz-> 40 50 60 70 80 90 100 110 120130 140 150 160 170 180 190 200 210 M Abundance #125731:2-(1 -METHYLINDOL-3'-YL)ETHENE-1,1 -DECARBONITRILE... 207 MNyMN UANNW 5000 ■ i ■ ■ ■ ‘ i ■ ■ r-j-r-r-n-j-r-r I 5.20 5.40 5.60 5.80 165 62 88 138 179 m/z 95.90 31.22% . 152

m/z-> 101 112 ..I.. . 0! "' i ■ • “ i ■ ‘ ■ ■ i " ‘ i" •11 ■ • 11’t L. 40 50 60 70 80 90 100 110120 130 140 150 160 170 180 190 200 210 Il 192 ■ | I I II | I I I I |II I I | 1 I I’T

Abundance #125674: Hexahydropyridine, 1-methyl-4-[4,5-dihydroxyphenyl]- 207 70 42 ■ i ■ ■ ‘ ‘ i ■ ■ ' ■ i

97 5.20 5.40 5.60 5.80 5000' m/z 208.00 28.46% 82 136 123 | 150 192 0! ’ ’1 ’ 1’4+414444 1 13013 TpmwmpT p-rT miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #125730: Pyrido[2,3-d]pyrimidine, 4-phenyl- $$ 4-Phenylpyr... ' 1 11 1 1 I 1 11 1 I 207 5.20 5.40 5.60 5.80 m/z 83.90 6.44% 5000 77 179 MWwAAMa/r 103 126 152 - 0 •‘'i‘“ i■11‘i1 ■ ■ ‘ i • ■ ‘ “11““i‘' I’r miz—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 5.20 5.40 5.60 5.80

01547.D HP022102.M Mon Feb 25 10:55:25 2002 Page 7

NYC-WTC_000010076

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GCMS analysis report for sample AE01511, March 2002 · Box DEP Box 14

NYC-WTC_000010047

GCMS laboratory results for sample AE01511 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

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