Laboratory report documenting GCMS analysis of a method blank for sample AE03615 to verify analytical system cleanliness.
NYC-WTC_000037760–000037779Folder label: “GCMS X 2/19/02 A 3/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report • Data File : C:\MSDCHEM\1\5973N\02MAR08\03615.D Vial: 5 Acq On : 8 Mar 2002 6:52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.
22.28 0.11 ug/L 88634 Phenanthrene-dl0 22.63
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 019169-94-9 72 192 C11H1203 2 N-perdeuteriobenzylideneaniline 000538-51-2 64 192 C13D11N 3 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-540 50 4 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2: 000000-00-0 46 Abundance Scan 1675 (22.283 min): 03515. D (-) m/z 192.00 100.00% 192
5000
oo 96 146 400 • ■ i ■ ■ 22.00 22.20 22.40 22.60 44 70 82 .1 118 0- ■■' I' " 'I'' ■' I " ■ ■ l ■'.' I' ■ '■ ill ■ ■! ■ H. 11 “ ' I “ ‘11 ‘ ‘' I ■'" I' I • "11 ‘ .1 160 .1 ' I' ■'' I" " I m/z 191.00 16.99% m/z—> 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192
108 5000 ’ 1/1/1/1/1/1/1.1 ■ i ■ ■ 22.00 22.20 22.40 22.60 146 175 m/z 96.10 14.32%
0 ■ ■ i •" ■ i ■ ■ • ■ i ■1 ■ • i ■ •" i “ ■' i ■ ■ ■ ■ i •1 ■ ‘ i'' i1 ■ ‘ ■ i “ “ i ■ “ ■ i ■ ■ • i • > • • i •»‘ • i ■ T m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192 ■ ■ i ‘ ■ i ■ ■ > । • ■ ■ > । ■ 22.00 22.20 22.40 22.60 5000 82 m/z 146.00 14.04% 54 110 30 94 160 0 - 1 ‘ i ■ “ ■ i ■ ■" i MP • •i1••*i• ■ ■ • i “ • • i • miz—> 2030405060 70 8090 .00 110 120 130 140 150 160 170 180 190 200 Tgr m Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospho!in... 159 192 22.00 22.20 22.40 22.60 m/z 193.00 13.47%
5000
144 177 * ,..........|....... — 0 ITTTIETIT’II mz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 2240 22.60
03515.D HP022102.M Fri Mar 15 10:09:31 2002 Page 15
NYC-WTC_000037778
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NYC-WTC_000037800
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03617 conducted on March 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037740
Laboratory report documenting GCMS analysis of a method blank for sample AE03614 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037635
Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037660
Laboratory report documenting GCMS analysis of a method blank for sample AE03509 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037680
Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037720
Laboratory report documenting GCMS analysis of a method blank for sample AE03612 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037700
Laboratory report documenting GCMS analysis of a method blank for sample AE03611 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052128
Laboratory report showing GCMS analysis of sample AE00843 including surrogate recovery and unknown compounds.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010027
GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.998
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Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
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