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GCMS surrogate recovery results for sample AE03184, March 2002

Machine-extracted title · confidence 100%

Analytical report showing surrogate recovery data for sample AE03184 analyzed on March 15, 2002.

NYC-WTC_000006045–000006064

Folder label: “GCMS X 2/12/02 A 3/01/02

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Scanned page image, NYC-WTC_000006062
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02MAR01\03184 .D Vial: 4 Acq On : 1 Mar 2002 12:48 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.12 ug/L 72108 Phenanthrene- dl 0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qua!

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H12O3 019169-94-9 72 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 53 3 1-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 4 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 47 Abundance Scan 1675 (22.283 min): 03184. D (-) m/z 192.00 100.00% 192

5000

82 96 146 160 . .......9..... .. aam l 118 22.00 22.20 22.40 22.60 ...........44......................... | m/z 191.00 17.71% 0 111"11 r' " i " ■ ■ i"111"1' i11" i ■111 111111*1adnadauu—* m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588: 4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 22.00 22.20 22.40 22.60 146 175 m/ z 96.00 17.37%

0 1II I' " ' i " " r 1 " r r " i " " i " " r 1 l1"' i" " r " 11" 11111111111 p 1...... 'I1 TT-p- m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 1912

22.00 22.20 22.40 22.60 5000 82 m/z 146.10 13.83% 54 110 30 160 — 0 —PT " i " " i' mH 1 94 " 11" " I Pri [ 1111111111....... .... 1111 ■ । rl1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospholin... ....................... A.................. , 159 192 22.00 22.20 22.40 22.60 m/z 193.00 13.47%

5000

144 177

0 " i ■ " 1 r " ■ i " " r ■ ■' i " " i ■ “ ' i " " i" ■ ■ i ■ ■" i " " r " 111111111 M H7 . ..... .. ..... 11 miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

>3184.D HP022102.M Mon Mar 04 12:32:53 2002 Page 14

NYC-WTC_000006062

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NYC-WTC_000006062Source: NYC Law Department, mirrored locally

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