GCMS analysis results for sample AE11926, June 2002

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Data File : C:\MSDCHEM\l\DATA\052302\11927.D Vial: 7 Acq On : 23 May 2002 2:51 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Dodecahydropyrido[1,2-b]iso... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

5.36 0.23 ug/L 144651 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Dodecahydropyrido[1,2-b]isoquino... 207 C13H21NO 1000195-30-7 >38 2 Piperidine 85 C5H11N 000110-89-4/10 3 Thiophene 84 C4H4S 000110-02-1 9 4 Thiophene 84 C4H4S 000110-02/1 9 Abundance Scan 389 (5.365 min): 11927.D (-385) (-) m/z 207.00 100.00% 2017 84

5000’

35 96 191 5.00 5.20 5.40 5.60 5.80

nz-> 0- ......... 0 20 1 4048....... 60 80 100 120 140 160 180 200 m/z 84.00 72.53% Abundance #84738: Dodecahydropyrido[1,2-b]isoquinolin-6-one 2017 84

5000 41 55 67 97 192 5.00 5.20 5.40 5.60 5.80 125 138 15 m/z 208.00 30.50% 182 164 178 109 29 0- 101111 4u—l4ull—l + L-, 14 miz-> 0 20 40 60 80 100 120 140 160 180 200 Abundance #116601: Piperidine 84 ■ ■ i ■ • • ■ i • ■ ■ i ■ ■ • ■ i ■ ' ■ ‘ i ‘ 500 5.20 5.40 5.60 5.80 50001 m/z 85.00 25.61% 56 29 44 70 0- 'I 1 ■ 1 1 i „al, s4l .. I., ■- tnfz-> 0 20 40 60I 80 100 120 140 160 180 200 Abundance #33732: Thiophene 84 500 5.20 5.40 5.60 5.80 m/z 96.30 20.95% 58 45 5000'

26 , 69

m/z-> 0 1 1 12 ! A -pluli 20 40 460— 80 " If -r-rTT-r-r-ry-r-r-r-r-p-T-T-T-Y-r-rT-r-!--^^ 100 120 140 160 180 200 ■ 1 i 1 ■ ■ ■ i ■ ■ 1 ■■i■• ■ ■ f 5.00 5.20 5.40 5.60 5.80

11927.D 052202.M Wed May 29 09:48:14 2002 Page 11

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