GCMS quantitation report, sample AE11933, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report • Data File : C:\MSDCHEM\1\DATA\0610022\11933.D Vial: 10 Acq On : 10 Jun 2002 6:21 pm Operator: Sample : gc/ms scan 6/7 fb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Thiophene Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 3.88 0.41 ug/L 335342 1,4-dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qua 1 Thiophene 84 C4H4S 000110-02-1 8 2 Thiophene 84 C4H4S 000110-02-19 3 Thiophene 84 C4H4S 000110-02-1 5 4 Piperidine 85 C5H11N 000110-89-4 5 Abundance Scan 136 (3.878 min): 11933.D (-134) (-) m/z 84.00 00.00% 84

5000 49 88 35 42 3.60 3.80 4.00 4.20 0- ----- TTTWTTTTTTTTTTTTTTT 11111 ‘ i" m/z 49.10 47.59% miz- > 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116584: Thiophene 84 58 45 5000 3.60 3.80 4.00 4.20 39 m/z 86.00 34.04% 26 32 50 69 0- 1111111111 n 11111111111 i-pn 1111111111111111 ++ ■ 11111 ■ । ■ 11 TTTTT miz-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116585: Thiophene 84

3.60 3.80 4.00 4.20 58 5000 m/z 84.95 27.71% 45 39

m/z—> 0- — 12 18 26 32 ,, 50 . ————— 11■11111■111 i[■ ■■ 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 „7.89H Abundance #33732: Thiophene 84 3.60 3.80 4.00 4.20

_M 58 m/z 88.00 26.13% 45 5000 39

1 12 26 32 1 50 1

m/z-> 0 ii 11111111111 ii । ■ Il ■ 11 ii 11 in 111111111 ri 1111 11111 0 ++H# 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ,. “1117189,1/788,,, ’ 173 3.60 3.80 4.00 4.20

11933.D 060302.M Tue Jun 11 08:23:09 2002 Page 9

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